5-amino-N,N'-bis[6-(3,3-dimethylbutyrylamino)pyridin-2-yl]-isophthalamide

Base Information

• Chemical Name: 5-amino-N,N'-bis[6-(3,3-dimethylbutyrylamino)pyridin-2-yl]-isophthalamide
• CAS No.: 717111-10-9
• Molecular Formula: C₃₀H₃₇N₇O₄
• Molecular Weight: 559.668

Synonyms:5-amino-N,N'-bis[6-(3,3-dimethylbutyrylamino)pyridin-2-yl]-isophthalamide

Chemical Property of 5-amino-N,N'-bis[6-(3,3-dimethylbutyrylamino)pyridin-2-yl]-isophthalamide

Chemical Property:

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Technology Process of 5-amino-N,N'-bis[6-(3,3-dimethylbutyrylamino)pyridin-2-yl]-isophthalamide

There total 5 articles about 5-amino-N,N'-bis[6-(3,3-dimethylbutyrylamino)pyridin-2-yl]-isophthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

N,N'-bis[6-(3,3-dimethylbutyrylamino)pyridin-2-yl]-5-nitro-isophthalamide (717111-02-9) → 5-amino-N,N'-bis[6-(3,3-dimethylbutyrylamino)pyridin-2-yl]-isophthalamide (717111-10-9)

Guidance literature:

With hydrogen; platinum(IV) oxide; In ethanol; at 20 ℃; for 24h; under 3000.24 Torr;

DOI:10.1002/chem.200305461

Reference yield:

3,3-dimethylbutanoic acid chloride (7065-46-5) → 5-amino-N,N'-bis[6-(3,3-dimethylbutyrylamino)pyridin-2-yl]-isophthalamide (717111-10-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 46 percent / Et₃N / tetrahydrofuran / 60 h / 20 °C

2: 97 percent / Et₃N / tetrahydrofuran / 12 h / 20 °C

3: 97 percent / H₂ / PtO₂*H₂O / ethanol / 24 h / 20 °C / 3000.24 Torr

With hydrogen; triethylamine; platinum(IV) oxide; In tetrahydrofuran; ethanol;

DOI:10.1002/chem.200305461

Reference yield:

2.6-diaminopyridine (141-86-6) → 5-amino-N,N'-bis[6-(3,3-dimethylbutyrylamino)pyridin-2-yl]-isophthalamide (717111-10-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 46 percent / Et₃N / tetrahydrofuran / 60 h / 20 °C

2: 97 percent / Et₃N / tetrahydrofuran / 12 h / 20 °C

3: 97 percent / H₂ / PtO₂*H₂O / ethanol / 24 h / 20 °C / 3000.24 Torr

With hydrogen; triethylamine; platinum(IV) oxide; In tetrahydrofuran; ethanol;

DOI:10.1002/chem.200305461

upstream raw materials:

N,N'-bis[6-(3,3-dimethylbutyrylamino)pyridin-2-yl]-5-nitro-isophthalamide

2.6-diaminopyridine

3,3-dimethylbutanoic acid chloride

5-nitro-1,3-benzenedicarbonylchloride

Downstream raw materials:

4,4-{di(6-aminohexanoic acid)-5-amino-N,N'-bis[6-(3,3-dimethylbutyricamino)pyridin-2-yl]isophthalamide-amide}-2,2'-bipyridine

5-(2,2':6',2''-terpyridine-4'-carboxamido)-N,N'-bis[6-(3,3-dimethylbutanamido)pyridin-2-yl]isophthalamide

5-[6-(2,2':6',2''-terpyridine-4'-carboxamido)hexanamido]-N,N'-bis[6-(3,3-dimethylbutanamido)pyridin-2-yl]isophthalamide

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