C₁₄H₁₃Cl₂NO₄

Base Information

Chemical Name:C₁₄H₁₃Cl₂NO₄
CAS No.:1268246-43-0
Molecular Formula:C₁₄H₁₃Cl₂NO₄
Molecular Weight:330.168
Hs Code.:

C<sub>14</sub>H<sub>13</sub>Cl<sub>2</sub>NO<sub>4</sub>

Synonyms:C₁₄H₁₃Cl₂NO₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₁₃Cl₂NO₄

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Technology Process of C₁₄H₁₃Cl₂NO₄

There total 6 articles about C₁₄H₁₃Cl₂NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1268246-42-9
C₁₄H₁₁Cl₂NO₄

: 1268246-43-0
C₁₄H₁₃Cl₂NO₄

Guidance literature:: C₁₄H₁₁Cl₂NO₄; With sodium tetrahydroborate; In ethanol; at 0 ℃; for 0.333333h;

With hydrogenchloride; water; In ethanol;

Reference yield:

: 83-38-5
2,6-dichlorobenzaldehyde

: 1268246-43-0
C₁₄H₁₃Cl₂NO₄

Guidance literature:: Multi-step reaction with 6 steps

1: hydroxylamine hydrochloride; sodium hydroxide / ethanol; water / 24 h / 90 °C

2: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 20 °C

3: sodium methylate / tetrahydrofuran / 16 h / 20 °C

4: N,N-dimethyl-formamide / 3 h / 110 °C

5: hydrogenchloride; silica gel / water; tetrahydrofuran / 1 h / 40 °C

6: sodium tetrahydroborate / ethanol / 0.33 h / 0 °C

With hydrogenchloride; sodium tetrahydroborate; N-chloro-succinimide; hydroxylamine hydrochloride; sodium methylate; silica gel; sodium hydroxide; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide;

Reference yield:

: 25185-95-9
2,6-dichlorobenzaldoxime

: 1268246-43-0
C₁₄H₁₃Cl₂NO₄

Guidance literature:: Multi-step reaction with 5 steps

1: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 20 °C

2: sodium methylate / tetrahydrofuran / 16 h / 20 °C

3: N,N-dimethyl-formamide / 3 h / 110 °C

4: hydrogenchloride; silica gel / water; tetrahydrofuran / 1 h / 40 °C

5: sodium tetrahydroborate / ethanol / 0.33 h / 0 °C

With hydrogenchloride; sodium tetrahydroborate; N-chloro-succinimide; sodium methylate; silica gel; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide;