3-(4-methoxyphenethyl)-3,6-dihydro-5-methoxy-1,4-bis(4-methoxyphenyl)pyrrolo[2,3-c]carbazol-7-ol

Base Information

Chemical Name:3-(4-methoxyphenethyl)-3,6-dihydro-5-methoxy-1,4-bis(4-methoxyphenyl)pyrrolo[2,3-c]carbazol-7-ol
CAS No.:900504-52-1
Molecular Formula:C₃₈H₃₄N₂O₅
Molecular Weight:598.698
Hs Code.:

Synonyms:3-(4-methoxyphenethyl)-3,6-dihydro-5-methoxy-1,4-bis(4-methoxyphenyl)pyrrolo[2,3-c]carbazol-7-ol

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Chemical Property of 3-(4-methoxyphenethyl)-3,6-dihydro-5-methoxy-1,4-bis(4-methoxyphenyl)pyrrolo[2,3-c]carbazol-7-ol

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Technology Process of 3-(4-methoxyphenethyl)-3,6-dihydro-5-methoxy-1,4-bis(4-methoxyphenyl)pyrrolo[2,3-c]carbazol-7-ol

There total 22 articles about 3-(4-methoxyphenethyl)-3,6-dihydro-5-methoxy-1,4-bis(4-methoxyphenyl)pyrrolo[2,3-c]carbazol-7-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1269631-74-4
7-(tert-butoxy)-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazole

: 900504-52-1
3-(4-methoxyphenethyl)-3,6-dihydro-5-methoxy-1,4-bis(4-methoxyphenyl)pyrrolo[2,3-c]carbazol-7-ol

Guidance literature:: With boron trichloride; In dichloromethane; pentamethylbenzene,; at -78 ℃;
DOI:10.1002/asia.201000544

Reference yield: 90.0%

: 7-(benzyloxy)-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazole

: 900504-52-1
3-(4-methoxyphenethyl)-3,6-dihydro-5-methoxy-1,4-bis(4-methoxyphenyl)pyrrolo[2,3-c]carbazol-7-ol

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethyl acetate; at 50 ℃; for 1h;
DOI:10.1002/ejoc.201402672

Reference yield:

: 1246523-44-3
2-azido-1-tert-butoxy-3-iodobenzene

: 900504-52-1
3-(4-methoxyphenethyl)-3,6-dihydro-5-methoxy-1,4-bis(4-methoxyphenyl)pyrrolo[2,3-c]carbazol-7-ol

Guidance literature:: Multi-step reaction with 3 steps

1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sodium hydroxide / 1,4-dioxane; water / 1.5 h / 20 °C

2: 1,2-dichloro-benzene / 0.5 h / Inert atmosphere; Reflux

3: boron trichloride / dichloromethane; pentamethylbenzene, / -78 °C

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; boron trichloride; sodium hydroxide; In 1,4-dioxane; dichloromethane; pentamethylbenzene,; water; 1,2-dichloro-benzene; 1: Suzuki-Miyaura coupling;
DOI:10.1002/asia.201000544