sulfuric acid 5-hydroxy-1,4-bis-(4-hydroxy-phenyl)-3-[2-(4-hydroxy-phenyl)-ethyl]-3,6-dihydropyrrolo[2,3-c]carbazol-7-yl ester 2,2,2-trichloro-ethyl ester

Base Information

Chemical Name:sulfuric acid 5-hydroxy-1,4-bis-(4-hydroxy-phenyl)-3-[2-(4-hydroxy-phenyl)-ethyl]-3,6-dihydropyrrolo[2,3-c]carbazol-7-yl ester 2,2,2-trichloro-ethyl ester
CAS No.:1269631-76-6
Molecular Formula:C₃₆H₂₇Cl₃N₂O₈S
Molecular Weight:754.044
Hs Code.:

sulfuric acid 5-hydroxy-1,4-bis-(4-hydroxy-phenyl)-3-[2-(4-hydroxy-phenyl)-ethyl]-3,6-dihydropyrrolo[2,3-c]carbazol-7-yl ester 2,2,2-trichloro-ethyl ester

Synonyms:sulfuric acid 5-hydroxy-1,4-bis-(4-hydroxy-phenyl)-3-[2-(4-hydroxy-phenyl)-ethyl]-3,6-dihydropyrrolo[2,3-c]carbazol-7-yl ester 2,2,2-trichloro-ethyl ester

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Chemical Property of sulfuric acid 5-hydroxy-1,4-bis-(4-hydroxy-phenyl)-3-[2-(4-hydroxy-phenyl)-ethyl]-3,6-dihydropyrrolo[2,3-c]carbazol-7-yl ester 2,2,2-trichloro-ethyl ester

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Technology Process of sulfuric acid 5-hydroxy-1,4-bis-(4-hydroxy-phenyl)-3-[2-(4-hydroxy-phenyl)-ethyl]-3,6-dihydropyrrolo[2,3-c]carbazol-7-yl ester 2,2,2-trichloro-ethyl ester

There total 23 articles about sulfuric acid 5-hydroxy-1,4-bis-(4-hydroxy-phenyl)-3-[2-(4-hydroxy-phenyl)-ethyl]-3,6-dihydropyrrolo[2,3-c]carbazol-7-yl ester 2,2,2-trichloro-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 3-(4-methoxyphenethyl)-3,6-dihydro-5-methoxy-1,4-bis(4-methoxyphenyl)pyrrolo[2,3-c]carbazol-7-yl 2,2,2-trichloroethyl sulfate

: 1269631-76-6
sulfuric acid 5-hydroxy-1,4-bis-(4-hydroxy-phenyl)-3-[2-(4-hydroxy-phenyl)-ethyl]-3,6-dihydropyrrolo[2,3-c]carbazol-7-yl ester 2,2,2-trichloro-ethyl ester

Guidance literature:: With boron trichloride; tetra-(n-butyl)ammonium iodide; In dichloromethane; at 0 - 20 ℃;
DOI:10.1002/asia.201000544

Reference yield:

: 1246523-44-3
2-azido-1-tert-butoxy-3-iodobenzene

: 1269631-76-6
sulfuric acid 5-hydroxy-1,4-bis-(4-hydroxy-phenyl)-3-[2-(4-hydroxy-phenyl)-ethyl]-3,6-dihydropyrrolo[2,3-c]carbazol-7-yl ester 2,2,2-trichloro-ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sodium hydroxide / 1,4-dioxane; water / 1.5 h / 20 °C

2: 1,2-dichloro-benzene / 0.5 h / Inert atmosphere; Reflux

3: boron trichloride / dichloromethane; pentamethylbenzene, / -78 °C

4: 1,4-diaza-bicyclo[2.2.2]octane / dichloromethane / 1 h / 20 °C

5: boron trichloride; tetra-(n-butyl)ammonium iodide / dichloromethane / 0 - 20 °C

With 1,4-diaza-bicyclo[2.2.2]octane; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; boron trichloride; tetra-(n-butyl)ammonium iodide; sodium hydroxide; In 1,4-dioxane; dichloromethane; pentamethylbenzene,; water; 1,2-dichloro-benzene; 1: Suzuki-Miyaura coupling;
DOI:10.1002/asia.201000544

Reference yield:

: 900504-52-1
3-(4-methoxyphenethyl)-3,6-dihydro-5-methoxy-1,4-bis(4-methoxyphenyl)pyrrolo[2,3-c]carbazol-7-ol

: 1269631-76-6
sulfuric acid 5-hydroxy-1,4-bis-(4-hydroxy-phenyl)-3-[2-(4-hydroxy-phenyl)-ethyl]-3,6-dihydropyrrolo[2,3-c]carbazol-7-yl ester 2,2,2-trichloro-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1,4-diaza-bicyclo[2.2.2]octane / dichloromethane / 1 h / 20 °C

2: boron trichloride; tetra-(n-butyl)ammonium iodide / dichloromethane / 0 - 20 °C

With 1,4-diaza-bicyclo[2.2.2]octane; boron trichloride; tetra-(n-butyl)ammonium iodide; In dichloromethane;
DOI:10.1002/asia.201000544