2-(2-(2,6-dichlorobenzylidene)hydrazinyl)-N’-(2,6-dichlorobenzylidene)-6-chloropyridine-4-carbohydrazide

Base Information

Chemical Name:2-(2-(2,6-dichlorobenzylidene)hydrazinyl)-N’-(2,6-dichlorobenzylidene)-6-chloropyridine-4-carbohydrazide
CAS No.:1422195-43-4
Molecular Formula:C₂₀H₁₂Cl₅N₅O
Molecular Weight:515.613
Hs Code.:

Synonyms:2-(2-(2,6-dichlorobenzylidene)hydrazinyl)-N’-(2,6-dichlorobenzylidene)-6-chloropyridine-4-carbohydrazide

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Chemical Property of 2-(2-(2,6-dichlorobenzylidene)hydrazinyl)-N’-(2,6-dichlorobenzylidene)-6-chloropyridine-4-carbohydrazide

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Technology Process of 2-(2-(2,6-dichlorobenzylidene)hydrazinyl)-N’-(2,6-dichlorobenzylidene)-6-chloropyridine-4-carbohydrazide

There total 4 articles about 2-(2-(2,6-dichlorobenzylidene)hydrazinyl)-N’-(2,6-dichlorobenzylidene)-6-chloropyridine-4-carbohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 2-chloro-6-hydrazinoisonicotinic acid hydrazide

: 83-38-5
2,6-dichlorobenzaldehyde

: 1422195-43-4
2-(2-(2,6-dichlorobenzylidene)hydrazinyl)-N’-(2,6-dichlorobenzylidene)-6-chloropyridine-4-carbohydrazide

Guidance literature:: In ethanol; for 6h; Reflux;
DOI:10.1007/s11164-013-1028-0

Reference yield:

: 5398-44-7
2,6-dichloropyridine-4-carboxylic acid

: 1422195-43-4
2-(2-(2,6-dichlorobenzylidene)hydrazinyl)-N’-(2,6-dichlorobenzylidene)-6-chloropyridine-4-carbohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid

2: hydrazine hydrate / ethanol / Reflux

3: ethanol / 6 h / Reflux

With sulfuric acid; hydrazine hydrate; In ethanol;
DOI:10.1007/s11164-013-1028-0

Reference yield:

: 99-11-6
citrazinic acid

: 1422195-43-4
2-(2-(2,6-dichlorobenzylidene)hydrazinyl)-N’-(2,6-dichlorobenzylidene)-6-chloropyridine-4-carbohydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: trichlorophosphate; triethylamine

2: sulfuric acid

3: hydrazine hydrate / ethanol / Reflux

4: ethanol / 6 h / Reflux

With sulfuric acid; hydrazine hydrate; triethylamine; trichlorophosphate; In ethanol;
DOI:10.1007/s11164-013-1028-0