bis(4-chlorophenyl)methyl bis(4-chlorophenyl)acetate

Base Information

• Chemical Name: bis(4-chlorophenyl)methyl bis(4-chlorophenyl)acetate
• CAS No.: 13144-34-8
• Molecular Formula: C27H18 Cl4 O2
• Molecular Weight: 516.251
• Mol file: 13144-34-8.mol

Synonyms:Aceticacid, bis(p-chlorophenyl)-, bis(p-chlorophenyl)methyl ester (8CI); Benzhydrol,4,4'-dichloro-, bis(p-chlorophenyl)acetate; NSC 406119

Chemical Property of bis(4-chlorophenyl)methyl bis(4-chlorophenyl)acetate

Chemical Property:

• Vapor Pressure: 1.03E-14mmHg at 25°C
• Boiling Point: 607.7°Cat760mmHg
• Flash Point: 198°C
• Density: 1.364g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of bis(4-chlorophenyl)methyl bis(4-chlorophenyl)acetate

There total 5 articles about bis(4-chlorophenyl)methyl bis(4-chlorophenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

formic acid (64-18-6) + 4,4'-dichlorobenzophenone (90-97-1) → bis(4'-chlorophenyl)acetic acid (83-05-6) + bis-(4-chloro-phenyl)-acetic acid-(4,4'-dichloro-benzhydryl ester) (13144-34-8)

Guidance literature:

With sulfuric acid; at 15 ℃; for 1.3h;

DOI:10.1246/cl.1985.1733

Reference yield: 2.0%

formic acid (64-18-6) + 4,4'-dichlorobenzophenone (90-97-1) → bis(4'-chlorophenyl)acetic acid (83-05-6) + bis-(4-chloro-phenyl)-acetic acid-(4,4'-dichloro-benzhydryl ester) (13144-34-8) + bis-4,4'-dichlorobenzhydryl ether (74562-99-5)

Guidance literature:

With sulfuric acid; at 15 ℃; for 1.3h; Product distribution; various diaryl methanol derivatives, effect of stirring;

DOI:10.1246/cl.1985.1733

Reference yield:

4,4'-dichlorobenzophenone (90-97-1) → bis-(4-chloro-phenyl)-acetic acid-(4,4'-dichloro-benzhydryl ester) (13144-34-8)

Guidance literature:

Multi-step reaction with 2 steps

1: Py

2: (thermolysis)

With pyridine;

DOI:10.1139/v67-492

upstream raw materials:

Oxalsaeure-bis-<4,4'-dichlor-benzhydryl-ester>

formic acid

4,4'-dichlorobenzophenone