(2S)-2-[(S)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-3-formylpropyl pivaloate

Base Information

Chemical Name:(2S)-2-[(S)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-3-formylpropyl pivaloate
CAS No.:865872-72-6
Molecular Formula:C₃₃H₅₀O₆Si
Molecular Weight:570.842
Hs Code.:

Synonyms:(2S)-2-[(S)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-3-formylpropyl pivaloate

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Chemical Property of (2S)-2-[(S)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-3-formylpropyl pivaloate

Chemical Property:

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Technology Process of (2S)-2-[(S)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-3-formylpropyl pivaloate

There total 6 articles about (2S)-2-[(S)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-3-formylpropyl pivaloate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2,2-dimethyl-propionic acid 2-[(4-benzyloxy-3-methoxy-phenyl)-triisopropylsilanyloxy-methyl]-4,5-dihydroxy-pentyl ester

: 865872-72-6
(2S)-2-[(S)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-3-formylpropyl pivaloate

Guidance literature:: With sodium periodate; In methanol; at 20 ℃; for 1h;
DOI:10.1271/bbb.69.113 DOI:10.1021/np050089s

Reference yield:

: 865872-70-4
(2S)-2-[(S)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-4-penten-1-ol

: 865872-72-6
(2S)-2-[(S)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-3-formylpropyl pivaloate

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / pyridine / CH₂Cl₂ / 2 h / 20 °C

2: OsO₄; 4-methylmorpholine N-oxide / H₂O; 2-methyl-propan-2-ol; acetone / 16 h / 20 °C

3: 13.6 g / NaIO₄ / methanol / 1 h / 20 °C

With pyridine; sodium periodate; osmium(VIII) oxide; 4-methylmorpholine N-oxide; In methanol; dichloromethane; water; acetone; tert-butyl alcohol;
DOI:10.1271/bbb.69.113

Reference yield:

: 865872-71-5
(4S,5S)-5-(4-benzyloxy-3-methoxyphenyl)-4-pivaloyloxymethyl-5-(triisopropylsilyloxy)-1-pentene

: 865872-72-6
(2S)-2-[(S)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-3-formylpropyl pivaloate

Guidance literature:: Multi-step reaction with 2 steps

1: OsO₄; 4-methylmorpholine N-oxide / H₂O; 2-methyl-propan-2-ol; acetone / 16 h / 20 °C

2: 13.6 g / NaIO₄ / methanol / 1 h / 20 °C

With sodium periodate; osmium(VIII) oxide; 4-methylmorpholine N-oxide; In methanol; water; acetone; tert-butyl alcohol;
DOI:10.1271/bbb.69.113