Zn((C(CH₃)3)2C₆H₃CC₄NH(O₃SCF₃)CHC₄NH(O₃SCF₃)C(C₆H₃(C(CH₃)3)2)C₄NH₂C(C₆H₃(C(CH₃)3)2)C₄NH₂)

Base Information

• Chemical Name: Zn((C(CH₃)3)2C₆H₃CC₄NH(O₃SCF₃)CHC₄NH(O₃SCF₃)C(C₆H₃(C(CH₃)3)2)C₄NH₂C(C₆H₃(C(CH₃)3)2)C₄NH₂)
• CAS No.: 947683-63-8
• Molecular Formula: C₆₄H₇₀F₆N₄O₆S₂Zn
• Molecular Weight: 1234.8

Synonyms:Zn((C(CH₃)3)2C₆H₃CC₄NH(O₃SCF₃)CHC₄NH(O₃SCF₃)C(C₆H₃(C(CH₃)3)2)C₄NH₂C(C₆H₃(C(CH₃)3)2)C₄NH₂)

Chemical Property of Zn((C(CH₃)3)2C₆H₃CC₄NH(O₃SCF₃)CHC₄NH(O₃SCF₃)C(C₆H₃(C(CH₃)3)2)C₄NH₂C(C₆H₃(C(CH₃)3)2)C₄NH₂)

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Technology Process of Zn((C(CH₃)3)2C₆H₃CC₄NH(O₃SCF₃)CHC₄NH(O₃SCF₃)C(C₆H₃(C(CH₃)3)2)C₄NH₂C(C₆H₃(C(CH₃)3)2)C₄NH₂)

There total 1 articles about Zn((C(CH₃)3)2C₆H₃CC₄NH(O₃SCF₃)CHC₄NH(O₃SCF₃)C(C₆H₃(C(CH₃)3)2)C₄NH₂C(C₆H₃(C(CH₃)3)2)C₄NH₂) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N-phenylbistrifluoromethane-sulfonimide (37595-74-7) + 2,18-bis(pinacolatoboryl)-5,10,15-tris(3,5-di-tert-butylphenyl)porphyrin + zinc diacetate (557-34-6) → Zn((C(CH3)3)2C6H3CC4NH(O3SCF3)CHC4NH(O3SCF3)C(C6H3(C(CH3)3)2)C4NH2C(C6H3(C(CH3)3)2)C4NH2) (947683-63-8)

Guidance literature:

With Oxone; Cs₂CO₃; In tetrahydrofuran; water; acetone; reaction with oxone in THF/acetone/H2O at room temp. for 1.5 h, then with C6H5N(O2SCF3)2, Cs2CO3 according to M. Oestreich et al. Angew. Chem. 2005, 117, 152 in DMF at room temp. for 12 h, then with Zn(CH3CO2)2 in CHCl3 and CH3OH at room temp. for 2 h;

DOI:10.1002/anie.200700550

Reference yield: 55.0%

Zn((C(CH3)3)2C6H3CC4NH(O3SCF3)CHC4NH(O3SCF3)C(C6H3(C(CH3)3)2)C4NH2C(C6H3(C(CH3)3)2)C4NH2) (947683-63-8) + diphenylphosphane (829-85-6) → C86H90N4P2Zn (1548823-89-7)

Guidance literature:

With palladium diacetate; triethylamine; 1,4-di(diphenylphosphino)-butane; In N,N-dimethyl-formamide; at 90 ℃; for 12h; Inert atmosphere;

DOI:10.1002/anie.201308551

Reference yield:

Zn((C(CH3)3)2C6H3CC4NH(O3SCF3)CHC4NH(O3SCF3)C(C6H3(C(CH3)3)2)C4NH2C(C6H3(C(CH3)3)2)C4NH2) (947683-63-8) + trimethylsilylacetylene (1066-54-2) → Zn((C(CH3)3)2C6H3CC4NH(C2Si(CH3)3)CHC4NH(C2Si(CH3)3)C(C6H3(C(CH3)3)2)C4NH2C(C6H3(C(CH3)3)2)C4NH2) (947683-67-2)

Guidance literature:

With Pd(P(C₆H₅)3)4; CuI; N(C₂H₅)3; In N,N-dimethyl-formamide; toluene; reaction at 70 °C for 3 h;

DOI:10.1002/anie.200700550

upstream raw materials:

N,N-phenylbistrifluoromethane-sulfonimide

zinc diacetate

Downstream raw materials:

Zn((C(CH₃)3)2C₆H₃CC₄NH(C₂Si(CH₃)3)CHC₄NH(C₂Si(CH₃)3)C(C₆H₃(C(CH₃)3)2)C₄NH₂C(C₆H₃(C(CH₃)3)2)C₄NH₂)

C₈₆H₉₀N₄P₂Zn

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