tert-butoxy 4-(2-(allyloxycarbamoyl)phenylcarbamoyl)pyridine-2,6-dicarboxylate

Base Information

Chemical Name:tert-butoxy 4-(2-(allyloxycarbamoyl)phenylcarbamoyl)pyridine-2,6-dicarboxylate
CAS No.:638128-24-2
Molecular Formula:C₂₆H₃₁N₃O₇
Molecular Weight:497.548
Hs Code.:

Synonyms:tert-butoxy 4-(2-(allyloxycarbamoyl)phenylcarbamoyl)pyridine-2,6-dicarboxylate

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Chemical Property of tert-butoxy 4-(2-(allyloxycarbamoyl)phenylcarbamoyl)pyridine-2,6-dicarboxylate

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Technology Process of tert-butoxy 4-(2-(allyloxycarbamoyl)phenylcarbamoyl)pyridine-2,6-dicarboxylate

There total 6 articles about tert-butoxy 4-(2-(allyloxycarbamoyl)phenylcarbamoyl)pyridine-2,6-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 2937-50-0
Allyl chloroformate

: 638128-23-1
tert-butoxy 4-(2-aminophenylcarbamoyl)pyridine-2,6-dicarboxylate

: 638128-24-2
tert-butoxy 4-(2-(allyloxycarbamoyl)phenylcarbamoyl)pyridine-2,6-dicarboxylate

Guidance literature:: With pyridine; dmap; In dichloromethane; at 20 ℃; for 2.5h;
DOI:10.1021/ja037895a

Reference yield:

: 138-60-3
chelidamic acid

: 638128-24-2
tert-butoxy 4-(2-(allyloxycarbamoyl)phenylcarbamoyl)pyridine-2,6-dicarboxylate

Guidance literature:: Multi-step reaction with 7 steps

1: POCl₃ / 12 h / 128 °C

2: 1.79 g / 4-dimethylaminopyridine; pyridine / CH₂Cl₂ / 16 h / 20 °C

3: 97 percent / NaN₃ / dimethylformamide / 24 h / 50 °C

4: 98 percent / Pd/C; H₂ / ethyl acetate; methanol / 12 h / 20 °C / 2585.74 Torr

5: 93 percent / 4-dimethylaminopyridine; pyridine / CH₂Cl₂ / 3 h / 20 °C

6: 95 percent / Pd/C; H₂ / ethyl acetate; methanol / 12 h / 20 °C / 2585.74 Torr

7: 82 percent / 4-dimethylaminopyridine; pyridine / CH₂Cl₂ / 2.5 h / 20 °C

With pyridine; dmap; palladium on activated charcoal; sodium azide; hydrogen; trichlorophosphate; In methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/ja037895a

Reference yield:

: 638128-21-9
tert-butoxy 4-aminopyridine-2,6-dicarboxylate

: 638128-24-2
tert-butoxy 4-(2-(allyloxycarbamoyl)phenylcarbamoyl)pyridine-2,6-dicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / 4-dimethylaminopyridine; pyridine / CH₂Cl₂ / 3 h / 20 °C

2: 95 percent / Pd/C; H₂ / ethyl acetate; methanol / 12 h / 20 °C / 2585.74 Torr

3: 82 percent / 4-dimethylaminopyridine; pyridine / CH₂Cl₂ / 2.5 h / 20 °C

With pyridine; dmap; palladium on activated charcoal; hydrogen; In methanol; dichloromethane; ethyl acetate;
DOI:10.1021/ja037895a