1,3-bis(2′,4′,6′-trimethylphenyl)imidazolium perchlorate

Base Information

• Chemical Name: 1,3-bis(2′,4′,6′-trimethylphenyl)imidazolium perchlorate
• CAS No.: 1259319-03-3
• Molecular Formula: C₂₁H₂₅N₂*ClO₄
• Molecular Weight: 404.894
• Mol file: 1259319-03-3.mol

Synonyms:1,3-bis(2′,4′,6′-trimethylphenyl)imidazolium perchlorate

Chemical Property of 1,3-bis(2′,4′,6′-trimethylphenyl)imidazolium perchlorate

Chemical Property:

Purity/Quality:

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Technology Process of 1,3-bis(2′,4′,6′-trimethylphenyl)imidazolium perchlorate

There total 2 articles about 1,3-bis(2′,4′,6′-trimethylphenyl)imidazolium perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

N,N'-bis(2,4,6-trimethylphenyl)ethanediimine (56222-36-7) + acetic acid (64-19-7,77671-22-8) → 1,3-bis(2′,4′,6′-trimethylphenyl)imidazolium perchlorate (1259319-03-3)

Guidance literature:

N,N'-bis(2,4,6-trimethylphenyl)ethanediimine; acetic acid; With perchloric acid; at 20 ℃;

In ethanol; Reflux;

DOI:10.1134/S1070363217120489

Reference yield: 10.0%

N,N'-bis(2,4,6-trimethylphenyl)ethanediimine (56222-36-7) → 1,3-bis(2′,4′,6′-trimethylphenyl)imidazolium perchlorate (1259319-03-3)

Guidance literature:

With perchloric acid; acetic acid; at 20 ℃;

DOI:10.1002/jhet.1847

Reference yield:

1,3-bis(2′,4′,6′-trimethylphenyl)imidazolium perchlorate (1259319-03-3) + (Z)-3-chloro-3-phenyl-2-propenal (33603-87-1) → C30H32ClN2O(1+)*ClO4(1-)

Guidance literature:

With triethylamine; In chloroform; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.1002/anie.202008631

upstream raw materials:

N,N'-bis(2,4,6-trimethylphenyl)ethanediimine

acetic acid