C₁₆H₇⁽²⁾H₇BrFN₂O

Base Information

Chemical Name:C₁₆H₇⁽²⁾H₇BrFN₂O
CAS No.:1287739-50-7
Molecular Formula:C₁₆H₁₄BrFN₂O
Molecular Weight:356.147
Hs Code.:

C<sub>16</sub>H<sub>7</sub><sup>(2)</sup>H<sub>7</sub>BrFN<sub>2</sub>O

Synonyms:C₁₆H₇⁽²⁾H₇BrFN₂O

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₆H₇⁽²⁾H₇BrFN₂O

Chemical Property:

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Technology Process of C₁₆H₇⁽²⁾H₇BrFN₂O

There total 6 articles about C₁₆H₇⁽²⁾H₇BrFN₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1287739-40-5
C₁₅H₇⁽²⁾H₃BrFN₂O

: 1287739-43-8
C₁₅H₆⁽²⁾H₄BrFN₂O

: 41251-37-0
methyl-d3-magnesium iodide

: 1287739-46-1
C₁₆H₈⁽²⁾H₆BrFN₂O

: 1287739-50-7
C₁₆H₇⁽²⁾H₇BrFN₂O

Guidance literature:: C₁₅H₇⁽²⁾H₃BrFN₂O; C₁₅H₆⁽²⁾H₄BrFN₂O; methyl-d3-magnesium iodide; In tetrahydrofuran; diethyl ether; Cooling in ice bath;

With water; ammonium chloride; In tetrahydrofuran; diethyl ether;

With potassium carbonate; In methanol; water; at 60 - 70 ℃;

Reference yield:

: 400-93-1
3-nitro-4-fluoroacetophenone

: 1287739-50-7
C₁₆H₇⁽²⁾H₇BrFN₂O

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1-methyl-pyrrolidin-2-one / 72 h / 90 °C

2.1: hydrogenchloride; ammonium chloride / iron / ethanol; water / 50 - 70 °C

3.1: 2 h / 80 °C

4.1: chloroform-d1; 2,3,4,6,7,8-hexahydro-1H-pyrimido[1,2-a]pyrimidine / 81 h / 20 - 60 °C

4.2: 70 °C

5.1: diethyl ether; tetrahydrofuran / Cooling in ice bath

5.3: 60 - 70 °C

With hydrogenchloride; chloroform-d1; 2,3,4,6,7,8-hexahydro-1H-pyrimido[1,2-a]pyrimidine; ammonium chloride; iron; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; diethyl ether; ethanol; water;

Reference yield:

: 1287739-75-6
1-(4-(3-bromo-4-fluorophenylamino)-3-nitrophenyl)-ethanone

: 1287739-50-7
C₁₆H₇⁽²⁾H₇BrFN₂O

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride; ammonium chloride / iron / ethanol; water / 50 - 70 °C

2.1: 2 h / 80 °C

3.1: chloroform-d1; 2,3,4,6,7,8-hexahydro-1H-pyrimido[1,2-a]pyrimidine / 81 h / 20 - 60 °C

3.2: 70 °C

4.1: diethyl ether; tetrahydrofuran / Cooling in ice bath

4.3: 60 - 70 °C

With hydrogenchloride; chloroform-d1; 2,3,4,6,7,8-hexahydro-1H-pyrimido[1,2-a]pyrimidine; ammonium chloride; iron; In tetrahydrofuran; diethyl ether; ethanol; water;