C₁₄H₇ClF₂N₂O

Base Information

Chemical Name:C₁₄H₇ClF₂N₂O
CAS No.:1588423-57-7
Molecular Formula:C₁₄H₇ClF₂N₂O
Molecular Weight:292.672
Hs Code.:

C<sub>14</sub>H<sub>7</sub>ClF<sub>2</sub>N<sub>2</sub>O

Synonyms:C₁₄H₇ClF₂N₂O

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Chemical Property of C₁₄H₇ClF₂N₂O

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Technology Process of C₁₄H₇ClF₂N₂O

There total 7 articles about C₁₄H₇ClF₂N₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 872046-08-7
(2,6-difluorophenyl)acetic acid methyl ester

: 1001756-21-3
4-amino-6-chloropyridine-3-carboxaldehyde

: 1588423-57-7
C₁₄H₇ClF₂N₂O

Guidance literature:: (2,6-difluorophenyl)acetic acid methyl ester; With sodium hydride; In tetrahydrofuran; mineral oil; at -78 ℃; for 0.5h;

4-amino-6-chloropyridine-3-carboxaldehyde; In tetrahydrofuran; mineral oil; at 20 ℃; for 16h;

Reference yield:

: 40296-46-6
ethyl 4,6-dichloronicotinate

: 1588423-57-7
C₁₄H₇ClF₂N₂O

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / acetonitrile / 16.5 h / 0 - 20 °C

2.1: trifluoroacetic acid / 16 h / Reflux

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / -78 °C

4.1: manganese(IV) oxide / tetrahydrofuran / 5 h / 20 °C

5.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / -78 °C

5.2: 16 h / 20 °C

With manganese(IV) oxide; lithium aluminium tetrahydride; sodium hydride; triethylamine; trifluoroacetic acid; In tetrahydrofuran; acetonitrile; mineral oil;

Reference yield:

: 1588423-42-0
ethyl 6-chloro-4-((2,4-dimethoxybenzyl)amino)nicotinate

: 1588423-57-7
C₁₄H₇ClF₂N₂O

Guidance literature:: Multi-step reaction with 4 steps

1.1: trifluoroacetic acid / 16 h / Reflux

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / -78 °C

3.1: manganese(IV) oxide / tetrahydrofuran / 5 h / 20 °C

4.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / -78 °C

4.2: 16 h / 20 °C

With manganese(IV) oxide; lithium aluminium tetrahydride; sodium hydride; trifluoroacetic acid; In tetrahydrofuran; mineral oil;