bis(diphenylstibino)dimethylgermane

Base Information

Chemical Name:bis(diphenylstibino)dimethylgermane
CAS No.:69561-93-9
Molecular Formula:C₂₆H₂₆GeSb₂
Molecular Weight:654.582
Hs Code.:

Synonyms:bis(diphenylstibino)dimethylgermane

Suppliers and Price of bis(diphenylstibino)dimethylgermane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of bis(diphenylstibino)dimethylgermane

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of bis(diphenylstibino)dimethylgermane

There total 1 articles about bis(diphenylstibino)dimethylgermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.4%

: 603-36-1
triphenylantimony

: 1529-48-2
dichlorodimethylgermanium

: 69561-93-9
bis(diphenylstibino)dimethylgermane

Guidance literature:: With lithium; In tetrahydrofuran; byproducts: LiC6H5; storing of SbPh3 with 20-fold excess of Li in THF for 20 h at room temp.under Ar, decanting from unreacted Li, sepn. of PhLi by addn. of t-C4H9Cl; dropwise addn. of Me2GeCl2 to soln. of intermediate Ph2SbLi at -10 to -30°C, evapn. of solvent; evapn., 3-fold extractn. with pentane, evapn. of pentane;

Reference yield: 69.0%

: 69561-93-9
bis(diphenylstibino)dimethylgermane

: 13463-39-3,71564-36-8
tetracarbonyl nickel

: 74823-50-0
catena-dicarbonyl-μ-[dimethylgermanium(diphenylstibine)]nickel

Guidance literature:: In pentane; byproducts: CO; (Ar); room temp.; stoichiometric amts.; solvent pumped off; stored under pentane for some h; elem. anal.;
DOI:10.1016/0022-1902(80)80078-9

Reference yield:

: 69561-93-9
bis(diphenylstibino)dimethylgermane

: 199620-14-9,13007-92-6
chromium⁽⁰⁾ hexacarbonyl

: 29985-15-7
((C₆H₅)3Sb)Cr(CO)5

Guidance literature:: In tetrahydrofuran; Irradiation (UV/VIS); (Ar); drowise addn. of (Ph2Sb)2GeMe2 to irradiated soln. of Cr(CO)6;
DOI:10.1016/0022-1902(80)80078-9