5α-cinnamoyloxy-9α,10β-(dimethylmethylenedioxy)-2α-hydroxytaxa-4(20),11-dien-13-one

Base Information

Chemical Name:5α-cinnamoyloxy-9α,10β-(dimethylmethylenedioxy)-2α-hydroxytaxa-4(20),11-dien-13-one
CAS No.:172304-02-8
Molecular Formula:C₃₂H₄₀O₆
Molecular Weight:520.666
Hs Code.:

Synonyms:5α-cinnamoyloxy-9α,10β-(dimethylmethylenedioxy)-2α-hydroxytaxa-4(20),11-dien-13-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5α-cinnamoyloxy-9α,10β-(dimethylmethylenedioxy)-2α-hydroxytaxa-4(20),11-dien-13-one

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Technology Process of 5α-cinnamoyloxy-9α,10β-(dimethylmethylenedioxy)-2α-hydroxytaxa-4(20),11-dien-13-one

There total 4 articles about 5α-cinnamoyloxy-9α,10β-(dimethylmethylenedioxy)-2α-hydroxytaxa-4(20),11-dien-13-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 2571-73-5
2α-acetoxy-5α-cinnamoyloxy-9α,10β-(dimethylmethylenedioxy)taxa-4(20),11-dien-13-one

: 477952-08-2
9α,10β-(dimethylmethylenedioxy)-2α,2α-dihydroxytaxa-4(20),11-dien-13-one

: 172304-02-8
5α-cinnamoyloxy-9α,10β-(dimethylmethylenedioxy)-2α-hydroxytaxa-4(20),11-dien-13-one

Guidance literature:: With potassium hydroxide; In 1,4-dioxane; methanol; at 0 - 20 ℃; for 4.5h;
DOI:10.1021/np020240n

Reference yield: 88.0%

: 2571-73-5
2α-acetoxy-5α-cinnamoyloxy-9α,10β-(dimethylmethylenedioxy)taxa-4(20),11-dien-13-one

: 172304-02-8
5α-cinnamoyloxy-9α,10β-(dimethylmethylenedioxy)-2α-hydroxytaxa-4(20),11-dien-13-one

Guidance literature:: With potassium hydroxide; In methanol;
DOI:10.1016/j.bmcl.2006.09.068

Reference yield:

: 3835-52-7
taxinine

: 172304-02-8
5α-cinnamoyloxy-9α,10β-(dimethylmethylenedioxy)-2α-hydroxytaxa-4(20),11-dien-13-one

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / aq. KOH / methanol

2: 88 percent / aq. KOH / methanol

With potassium hydroxide; In methanol;
DOI:10.1016/j.bmcl.2006.09.068