3-Hydroxy-3-methyl-pentanedioic acid (1R,2R,3R,5S)-3-[(E)-3-(3,4-dimethoxy-phenyl)-acryloyloxy]-2,5-dihydroxy-5-methoxycarbonyl-cyclohexyl ester methyl ester

Base Information

• Chemical Name: 3-Hydroxy-3-methyl-pentanedioic acid (1R,2R,3R,5S)-3-[(E)-3-(3,4-dimethoxy-phenyl)-acryloyloxy]-2,5-dihydroxy-5-methoxycarbonyl-cyclohexyl ester methyl ester
• CAS No.: 103744-78-1
• Molecular Formula: C₂₆H₃₄O₁₃
• Molecular Weight: 554.548

Synonyms:3-Hydroxy-3-methyl-pentanedioic acid (1R,2R,3R,5S)-3-[(E)-3-(3,4-dimethoxy-phenyl)-acryloyloxy]-2,5-dihydroxy-5-methoxycarbonyl-cyclohexyl ester methyl ester

Chemical Property of 3-Hydroxy-3-methyl-pentanedioic acid (1R,2R,3R,5S)-3-[(E)-3-(3,4-dimethoxy-phenyl)-acryloyloxy]-2,5-dihydroxy-5-methoxycarbonyl-cyclohexyl ester methyl ester

Chemical Property:

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Technology Process of 3-Hydroxy-3-methyl-pentanedioic acid (1R,2R,3R,5S)-3-[(E)-3-(3,4-dimethoxy-phenyl)-acryloyloxy]-2,5-dihydroxy-5-methoxycarbonyl-cyclohexyl ester methyl ester

There total 5 articles about 3-Hydroxy-3-methyl-pentanedioic acid (1R,2R,3R,5S)-3-[(E)-3-(3,4-dimethoxy-phenyl)-acryloyloxy]-2,5-dihydroxy-5-methoxycarbonyl-cyclohexyl ester methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetramethylether of 3,5-di-O-caffeoyl-4-O-(3-hydroxy-3-methyl)glutaroylquinic acid dimethyl ester (114653-47-3) → dimethyl 3-hydroxy-3-methylglutarate (56652-39-2) + methyl (E)-3-(3,4-dimethoxyphenyl)acrylate (5396-64-5) + di-O-methylchlorogenic acid methyl ester (103744-79-2,123410-66-2) + 3-Hydroxy-3-methyl-pentanedioic acid (1R,2R,3R,5S)-3-[(E)-3-(3,4-dimethoxy-phenyl)-acryloyloxy]-2,5-dihydroxy-5-methoxycarbonyl-cyclohexyl ester methyl ester (103744-78-1)

Guidance literature:

With hydrogenchloride; for 3h; Heating;

DOI:10.1248/cpb.36.87

Reference yield:

3,4-dicaffeoyl-5-(3-hydroxy-3-methylglutaroyl)quinic acid hexamethylate → dimethyl 3-hydroxy-3-methylglutarate (56652-39-2) + methyl (E)-3-(3,4-dimethoxyphenyl)acrylate (5396-64-5) + di-O-methylchlorogenic acid methyl ester (103744-79-2,123410-66-2) + 3-Hydroxy-3-methyl-pentanedioic acid (1R,2R,3R,5S)-3-[(E)-3-(3,4-dimethoxy-phenyl)-acryloyloxy]-2,5-dihydroxy-5-methoxycarbonyl-cyclohexyl ester methyl ester (103744-78-1)

Guidance literature:

With hydrogenchloride; methanol;

DOI:10.1248/cpb.34.1419

Reference yield:

methanol (67-56-1) + tetramethylether of 3,5-di-O-caffeoyl-4-O-(3-hydroxy-3-methyl)glutaroylquinic acid dimethyl ester (114653-47-3) → dimethyl 3-hydroxy-3-methylglutarate (56652-39-2) + methyl (E)-3-(3,4-dimethoxyphenyl)acrylate (5396-64-5) + di-O-methylchlorogenic acid methyl ester (103744-79-2,123410-66-2) + 3-Hydroxy-3-methyl-pentanedioic acid (1R,2R,3R,5S)-3-[(E)-3-(3,4-dimethoxy-phenyl)-acryloyloxy]-2,5-dihydroxy-5-methoxycarbonyl-cyclohexyl ester methyl ester (103744-78-1)

Guidance literature:

With hydrogenchloride; for 3h; Heating;

DOI:10.1248/cpb.36.87

upstream raw materials:

methanol

tetramethylether of 3,5-di-O-caffeoyl-4-O-(3-hydroxy-3-methyl)glutaroylquinic acid dimethyl ester

3,5-di-O-caffeoyl-4-O-(3-hydroxy-3-methyl)glutaroylquinic acid

3,5-di-O-caffeoyl-4-O-(3-hydroxy-3-methyl)glutaroylquinic acid dimethyl ester

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