3-bromo-4-fluorobenzyl metanesulfonate

Base Information Edit

Chemical Name:3-bromo-4-fluorobenzyl metanesulfonate
CAS No.:866862-23-9
Molecular Formula:C₈H₈BrFO₃S
Molecular Weight:283.118
Hs Code.:
Mol file:866862-23-9.mol

Synonyms:3-bromo-4-fluorobenzyl metanesulfonate

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Chemical Property of 3-bromo-4-fluorobenzyl metanesulfonate Edit

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Technology Process of 3-bromo-4-fluorobenzyl metanesulfonate

There total 2 articles about 3-bromo-4-fluorobenzyl metanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 77771-03-0
3-bromo-4-fluoro-benzyl alcohol

: 124-63-0
methanesulfonyl chloride

: 866862-23-9
3-bromo-4-fluorobenzyl metanesulfonate

Guidance literature:: With triethylamine; In dichloromethane; at -20 - 20 ℃;
DOI:10.1021/jm200866y

Reference yield:

: 77771-02-9
3-bromo-4-fluorobenzaldehyde

: 866862-23-9
3-bromo-4-fluorobenzyl metanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 1 h / 0 °C

2: triethylamine / dichloromethane / 0.5 h / 0 °C

With sodium tetrahydroborate; triethylamine; In methanol; dichloromethane;