dimethyl 2-(benzyloxy)-5-formylphenylphosphonate

Base Information

Chemical Name:dimethyl 2-(benzyloxy)-5-formylphenylphosphonate
CAS No.:153886-98-7
Molecular Formula:C₁₆H₁₇O₅P
Molecular Weight:320.282
Hs Code.:

Synonyms:dimethyl 2-(benzyloxy)-5-formylphenylphosphonate

Suppliers and Price of dimethyl 2-(benzyloxy)-5-formylphenylphosphonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of dimethyl 2-(benzyloxy)-5-formylphenylphosphonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of dimethyl 2-(benzyloxy)-5-formylphenylphosphonate

There total 7 articles about dimethyl 2-(benzyloxy)-5-formylphenylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 153886-97-6
dimethyl 2-(benzyloxy)-5-(hydroxymethyl)phenylphosphonate

: 153886-98-7
dimethyl 2-(benzyloxy)-5-formylphenylphosphonate

Guidance literature:: With manganese(IV) oxide; In tetrahydrofuran; for 1.5h; Ambient temperature;
DOI:10.1002/hlca.19930760706

Reference yield:

: 623-05-2
(4-hydroxyphenyl)methanol

: 153886-98-7
dimethyl 2-(benzyloxy)-5-formylphenylphosphonate

Guidance literature:: Multi-step reaction with 6 steps

1: 87 percent / 1H-imidazole / dimethylformamide / 48 h / Ambient temperature

3: 77 percent / LDA / tetrahydrofuran / 1 h / -78 °C

4: 1.) NaH; 2.) MgBr₂ / 1.) THF, 0 deg C, 30 min; 2.) DMF, 15 h, room temp.

5: 85 percent / Bu₄NF / tetrahydrofuran / 0.42 h / 20 °C

6: 96 percent / MnO₂ / tetrahydrofuran / 1.5 h / Ambient temperature

With 1H-imidazole; manganese(IV) oxide; tetrabutyl ammonium fluoride; sodium hydride; magnesium bromide; lithium diisopropyl amide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19930760706

Reference yield:

: 100-39-0
benzyl bromide

: 153886-98-7
dimethyl 2-(benzyloxy)-5-formylphenylphosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH; 2.) MgBr₂ / 1.) THF, 0 deg C, 30 min; 2.) DMF, 15 h, room temp.

2: 85 percent / Bu₄NF / tetrahydrofuran / 0.42 h / 20 °C

3: 96 percent / MnO₂ / tetrahydrofuran / 1.5 h / Ambient temperature

With manganese(IV) oxide; tetrabutyl ammonium fluoride; sodium hydride; magnesium bromide; In tetrahydrofuran;
DOI:10.1002/hlca.19930760706