[HP(i-PrNCH₂CH₂)3N][Al(phenoxido)(tris(2-oxy-3,5-dimethylbenzyl)amine)]

Base Information

• Chemical Name: [HP(i-PrNCH₂CH₂)3N][Al(phenoxido)(tris(2-oxy-3,5-dimethylbenzyl)amine)]
• CAS No.: 915980-27-7
• Molecular Formula: C₁₅H₃₄N₄P*C₃₃H₃₅AlNO₄
• Molecular Weight: 838.062
• Mol file: 915980-27-7.mol

Synonyms:[HP(i-PrNCH₂CH₂)3N][Al(phenoxido)(tris(2-oxy-3,5-dimethylbenzyl)amine)]

Chemical Property of [HP(i-PrNCH₂CH₂)3N][Al(phenoxido)(tris(2-oxy-3,5-dimethylbenzyl)amine)]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [HP(i-PrNCH₂CH₂)3N][Al(phenoxido)(tris(2-oxy-3,5-dimethylbenzyl)amine)]

There total 1 articles about [HP(i-PrNCH₂CH₂)3N][Al(phenoxido)(tris(2-oxy-3,5-dimethylbenzyl)amine)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

(Al(tris(2-oxy-3,5-dimethylbenzyl)amine))2 (915980-22-2) + 2,5,8,9-tetraaza-1-phosphabicyclo[3.3.3]undecane 2,8,9-tris(1-methylethyl) (175845-21-3) + phenol (108-95-2,27073-41-2) → [HP(i-PrNCH2CH2)3N][Al(phenoxido)(tris(2-oxy-3,5-dimethylbenzyl)amine)] (915980-27-7)

Guidance literature:

In dichloromethane; toluene; under Ar; soln. of phenol and tri-isopropylproazaphosphatrane in tolueneadded to suspn. of Al complex in CH2Cl2, mixt. stirred at room temp. fo r 3 h; volatiles removed under vac.; elem. anal.;

DOI:10.1021/ja0626786

Reference yield:

dichloromethane (75-09-2) + [HP(i-PrNCH2CH2)3N][Al(phenoxido)(tris(2-oxy-3,5-dimethylbenzyl)amine)] (915980-27-7) → [HP(i-PrNCH2CH2)3N][Al(phenoxido)(tris(2-oxy-3,5-dimethylbenzyl)amine)] * dichloromethane

Guidance literature:

In dichloromethane; toluene; pentane; crystn. from toluene/CH2Cl2/pentane (1/1/6);

DOI:10.1021/ja0626786

upstream raw materials:

(Al(tris(2-oxy-3,5-dimethylbenzyl)amine))2

2,5,8,9-tetraaza-1-phosphabicyclo[3.3.3]undecane 2,8,9-tris(1-methylethyl)

phenol