tert-butyl (1S,2R)-2-(4-methoxybenzylamino)-1-(4-methoxyphenyl) propylcarbamate

Base Information

Chemical Name:tert-butyl (1S,2R)-2-(4-methoxybenzylamino)-1-(4-methoxyphenyl) propylcarbamate
CAS No.:1276021-56-7
Molecular Formula:C₂₃H₃₂N₂O₄
Molecular Weight:400.518
Hs Code.:

Synonyms:tert-butyl (1S,2R)-2-(4-methoxybenzylamino)-1-(4-methoxyphenyl) propylcarbamate

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Chemical Property of tert-butyl (1S,2R)-2-(4-methoxybenzylamino)-1-(4-methoxyphenyl) propylcarbamate

Chemical Property:

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Technology Process of tert-butyl (1S,2R)-2-(4-methoxybenzylamino)-1-(4-methoxyphenyl) propylcarbamate

There total 6 articles about tert-butyl (1S,2R)-2-(4-methoxybenzylamino)-1-(4-methoxyphenyl) propylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1252676-24-6
tert-butyl (1S,2R)-2-amino-1-(4-methoxyphenyl)propylcarbamate

: 123-11-5
4-methoxy-benzaldehyde

: 1276021-56-7
tert-butyl (1S,2R)-2-(4-methoxybenzylamino)-1-(4-methoxyphenyl) propylcarbamate

Guidance literature:: tert-butyl (1S,2R)-2-amino-1-(4-methoxyphenyl)propylcarbamate; 4-methoxy-benzaldehyde; In ethanol; at 20 ℃; for 4h;

With sodium tetrahydroborate; In ethanol; at 0 - 20 ℃; for 14h;

With ammonium chloride; In ethanol; water;

Reference yield:

: 4180-23-8,25086-72-0,63589-56-0
E-1-(4'-methoxyphenyl)prop-1-ene

: 1276021-56-7
tert-butyl (1S,2R)-2-(4-methoxybenzylamino)-1-(4-methoxyphenyl) propylcarbamate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydroxide / water; propan-1-ol / 0.08 h / 20 °C

1.2: 0.17 h / 20 °C

1.3: 0 °C

2.1: triethylamine / dichloromethane / 18 h / 0 - 20 °C

3.1: sodium azide / N,N-dimethyl-formamide / 2 h / 70 °C

4.1: hydrogen / palladium 10% on activated carbon / ethanol / 24 h / 20 °C / 3000.3 Torr / Inert atmosphere

5.1: ethanol / 4 h / 20 °C

5.2: 14 h / 0 - 20 °C

With sodium azide; hydrogen; triethylamine; sodium hydroxide; palladium 10% on activated carbon; In propan-1-ol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 4248-19-5
tert-butyl carbazate

: 1276021-56-7
tert-butyl (1S,2R)-2-(4-methoxybenzylamino)-1-(4-methoxyphenyl) propylcarbamate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydroxide / water; propan-1-ol / 0.08 h / 20 °C

1.2: 0.17 h / 20 °C

1.3: 0 °C

2.1: triethylamine / dichloromethane / 18 h / 0 - 20 °C

3.1: sodium azide / N,N-dimethyl-formamide / 2 h / 70 °C

4.1: hydrogen / palladium 10% on activated carbon / ethanol / 24 h / 20 °C / 3000.3 Torr / Inert atmosphere

5.1: ethanol / 4 h / 20 °C

5.2: 14 h / 0 - 20 °C

With sodium azide; hydrogen; triethylamine; sodium hydroxide; palladium 10% on activated carbon; In propan-1-ol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;