4-(2-(2-(2-methanesulfonyloxyethoxy)ethoxy)ethoxy)-3-methoxybenzaldehyde

Base Information

Chemical Name:4-(2-(2-(2-methanesulfonyloxyethoxy)ethoxy)ethoxy)-3-methoxybenzaldehyde
CAS No.:1338227-38-5
Molecular Formula:C₁₅H₂₂O₈S
Molecular Weight:362.401
Hs Code.:

Synonyms:4-(2-(2-(2-methanesulfonyloxyethoxy)ethoxy)ethoxy)-3-methoxybenzaldehyde

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Chemical Property of 4-(2-(2-(2-methanesulfonyloxyethoxy)ethoxy)ethoxy)-3-methoxybenzaldehyde

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Technology Process of 4-(2-(2-(2-methanesulfonyloxyethoxy)ethoxy)ethoxy)-3-methoxybenzaldehyde

There total 2 articles about 4-(2-(2-(2-methanesulfonyloxyethoxy)ethoxy)ethoxy)-3-methoxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.7%

: 1338227-36-3
4-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)-3-methoxybenzaldehyde

: 124-63-0
methanesulfonyl chloride

: 1338227-38-5
4-(2-(2-(2-methanesulfonyloxyethoxy)ethoxy)ethoxy)-3-methoxybenzaldehyde

Guidance literature:: 4-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)-3-methoxybenzaldehyde; With triethylamine; In dichloromethane; at 20 ℃; for 1h;

methanesulfonyl chloride; In dichloromethane; at 0 - 20 ℃;
DOI:10.1016/j.bmcl.2011.08.003

Reference yield:

: 5197-62-6
2-[2-(chloroethoxy)ethoxy]ethanol

: 1338227-38-5
4-(2-(2-(2-methanesulfonyloxyethoxy)ethoxy)ethoxy)-3-methoxybenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: N,N-dimethyl-formamide / 5 h / 100 °C

2.1: triethylamine / dichloromethane / 1 h / 20 °C

2.2: 0 - 20 °C

With triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.08.003