methyl N-phenylacetimidate

Base Information

• Chemical Name: methyl N-phenylacetimidate
• CAS No.: 55504-04-6
• Molecular Formula: C₉H₁₁NO
• Molecular Weight: 149.192
• Mol file: 55504-04-6.mol

Synonyms:methyl N-phenylacetimidate

Chemical Property of methyl N-phenylacetimidate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methyl N-phenylacetimidate

There total 6 articles about methyl N-phenylacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

sodium methylate (124-41-4) + (E)-N-(1-(1H-benzo[d][1,2,3]triazol-1-yl)ethylidene)aniline (161768-52-1) → methyl N-phenylacetimidate (55504-04-6)

Guidance literature:

In methanol; for 16h; Heating;

Reference yield: 72.0%

methanol (67-56-1) + Acetanilidoxim (5661-30-3) → methyl N-phenylacetimidate (55504-04-6)

Guidance literature:

With potassium hydroxide; at 15 ℃; Electrochemical reaction;

DOI:10.1246/bcsj.76.427

Reference yield:

cis-azobenzene (1080-16-6) → methyl N-phenylacetimidate (55504-04-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) (CO)5Cr=C(OMe)Me, 2.) methanol / 1.) hexane, r.t., 2.5 h, 2.) r.t., 14 h

2: 1.) hexane, r.t., 1h, 2.) r.t., 5 h; 60 deg C, 24 h

With methanol; pentacarbonyl(methoxymethylcarbene)chromium⁽⁰⁾;

DOI:10.1021/ja00208a010

upstream raw materials:

sodium methylate

(E)-N-(1-(1H-benzo[d][1,2,3]triazol-1-yl)ethylidene)aniline

trans-azobenzene

methanol