zinc 2-carboxyl-29H,31H-phthalocyanine

Base Information

Chemical Name:zinc 2-carboxyl-29H,31H-phthalocyanine
CAS No.:912562-84-6
Molecular Formula:C₃₃H₁₆N₈O₂Zn
Molecular Weight:621.932
Hs Code.:

Synonyms:zinc 2-carboxyl-29H,31H-phthalocyanine

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Chemical Property of zinc 2-carboxyl-29H,31H-phthalocyanine

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Technology Process of zinc 2-carboxyl-29H,31H-phthalocyanine

There total 1 articles about zinc 2-carboxyl-29H,31H-phthalocyanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85-44-9
phthalic anhydride

: 557-34-6
zinc diacetate

: 57-13-6
urea

: 552-30-7,145253-53-8
trimellitic Anhydride

: 14320-04-8
zinc(II) phthalocyanine

: 912562-84-6
zinc 2-carboxyl-29H,31H-phthalocyanine

Guidance literature:: With potassium hydroxide; ammonium molybdate; ammonium chloride; In not given; byproducts: polycarboxy substituted phtalocyanine zinc; trimellitic anhydride and phthalic anhydride (1:7) in presence of urea, zinc acetate and ammonium molybdate reacted at 170°C for 4 h; mixture then hydrolysed under alkaline condition; purified by HPLC column chromy. (silica gel/DMF:acetone (3:1));
DOI:10.1016/j.inoche.2005.12.002

Reference yield:

: 912562-84-6
zinc 2-carboxyl-29H,31H-phthalocyanine

: GGGFLG-[D-Lys⁶]-GnRH

: C₁₁₅H₁₃₀N₃₂O₂₀Zn

Guidance literature:: zinc 2-carboxyl-29H,31H-phthalocyanine; With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

GGGFLG-[D-Lys⁶]-GnRH; In N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1021/acs.jmedchem.7b01216