ethyl 2,3,4-tri-O-benzyl-6-O-(2,2'-bipyridin-6-yl)-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:ethyl 2,3,4-tri-O-benzyl-6-O-(2,2'-bipyridin-6-yl)-1-thio-β-D-glucopyranoside
CAS No.:1200396-63-9
Molecular Formula:C₃₉H₄₀N₂O₅S
Molecular Weight:648.823
Hs Code.:

Synonyms:ethyl 2,3,4-tri-O-benzyl-6-O-(2,2'-bipyridin-6-yl)-1-thio-β-D-glucopyranoside

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Chemical Property of ethyl 2,3,4-tri-O-benzyl-6-O-(2,2'-bipyridin-6-yl)-1-thio-β-D-glucopyranoside

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Technology Process of ethyl 2,3,4-tri-O-benzyl-6-O-(2,2'-bipyridin-6-yl)-1-thio-β-D-glucopyranoside

There total 1 articles about ethyl 2,3,4-tri-O-benzyl-6-O-(2,2'-bipyridin-6-yl)-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 39483-51-7,119645-03-3,128850-50-0,126461-54-9
ethyl 2,3,4-tri-O-benzyl-1-thio-β-D-glucopyranoside

: 13040-77-2
6-Chloro-[2,2']bipyridinyl

: 1200396-63-9
ethyl 2,3,4-tri-O-benzyl-6-O-(2,2'-bipyridin-6-yl)-1-thio-β-D-glucopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃;
DOI:10.1039/b903942b

Reference yield: 76.0%

: 53008-65-4,641635-63-4
methyl 2,3,4-tri-O-benzyl-D-glucopyranoside

: 1200396-63-9
ethyl 2,3,4-tri-O-benzyl-6-O-(2,2'-bipyridin-6-yl)-1-thio-β-D-glucopyranoside

: C₆₆H₆₈N₂O₁₁

Guidance literature:: With dimethyl-(methylthio)-sulphonium trifluoromethanesulphonate; In 1,2-dichloro-ethane; for 4h; Molecular sieve; Inert atmosphere;
DOI:10.1039/b903942b

Reference yield: 48.0%

: 1200396-63-9
ethyl 2,3,4-tri-O-benzyl-6-O-(2,2'-bipyridin-6-yl)-1-thio-β-D-glucopyranoside

: 71591-75-8
sodium 2-mercaptothiazolinate

: 1200396-64-0
2-thiazolinyl 2,3,4,-tri-O-benzyl-6-O-(2,2'-bipyridin-6-yl)-1-thio-β-D-glucopyranoside

Guidance literature:: ethyl 2,3,4-tri-O-benzyl-6-O-(2,2'-bipyridin-6-yl)-1-thio-β-D-glucopyranoside; With bromine; In dichloromethane; at 20 ℃; Molecular sieve; Inert atmosphere;

sodium 2-mercaptothiazolinate; In acetonitrile; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1039/b903942b