2-thiazolinyl 2,3,4,-tri-O-benzyl-6-O-(2,2'-bipyridin-6-yl)-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:2-thiazolinyl 2,3,4,-tri-O-benzyl-6-O-(2,2'-bipyridin-6-yl)-1-thio-β-D-glucopyranoside
CAS No.:1200396-64-0
Molecular Formula:C₄₀H₃₉N₃O₅S₂
Molecular Weight:705.899
Hs Code.:

Synonyms:2-thiazolinyl 2,3,4,-tri-O-benzyl-6-O-(2,2'-bipyridin-6-yl)-1-thio-β-D-glucopyranoside

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Chemical Property of 2-thiazolinyl 2,3,4,-tri-O-benzyl-6-O-(2,2'-bipyridin-6-yl)-1-thio-β-D-glucopyranoside

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Technology Process of 2-thiazolinyl 2,3,4,-tri-O-benzyl-6-O-(2,2'-bipyridin-6-yl)-1-thio-β-D-glucopyranoside

There total 1 articles about 2-thiazolinyl 2,3,4,-tri-O-benzyl-6-O-(2,2'-bipyridin-6-yl)-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1200396-63-9
ethyl 2,3,4-tri-O-benzyl-6-O-(2,2'-bipyridin-6-yl)-1-thio-β-D-glucopyranoside

: 71591-75-8
sodium 2-mercaptothiazolinate

: 1200396-64-0
2-thiazolinyl 2,3,4,-tri-O-benzyl-6-O-(2,2'-bipyridin-6-yl)-1-thio-β-D-glucopyranoside

Guidance literature:: ethyl 2,3,4-tri-O-benzyl-6-O-(2,2'-bipyridin-6-yl)-1-thio-β-D-glucopyranoside; With bromine; In dichloromethane; at 20 ℃; Molecular sieve; Inert atmosphere;

sodium 2-mercaptothiazolinate; In acetonitrile; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1039/b903942b

Reference yield: 60.0%

: 14104-20-2
silver tetrafluoroborate

: 1200396-64-0
2-thiazolinyl 2,3,4,-tri-O-benzyl-6-O-(2,2'-bipyridin-6-yl)-1-thio-β-D-glucopyranoside

: fac-[(PtMe₃I)4]

: 67-64-1
acetone

: fac-[PtMe3(2-thiazolinyl 2,3,4-tri-O-benzyl-6-O-(2,2'-bipyridine-6-yl)-1-thio-β-D-glucopyranoside)][BF4]

Guidance literature:: In acetone; byproducts: AgI; under Ar; a suspn. of Pt-contg. compd. (0.04 mmol) and AgBF4 (0.14 mmol)in acetone was stirred for 30 min under the absence of light; AgI was r emoved by filtration; a soln. of Pt-contg. compd. was added to the ligand (0.14 mmol); after 5 h the vol. of the soln. was reduced in vac. and pentane was added; the solid was filtered, washed with pentane and dried in vac.;
DOI:10.1039/b927058b