2,4-dinitrobenzylidene diacetate

Base Information

• Chemical Name: 2,4-dinitrobenzylidene diacetate
• CAS No.: 1500090-76-5
• Molecular Formula: C₁₁H₁₀N₂O₈
• Molecular Weight: 298.209
• Mol file: 1500090-76-5.mol

Synonyms:2,4-dinitrobenzylidene diacetate

Chemical Property of 2,4-dinitrobenzylidene diacetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,4-dinitrobenzylidene diacetate

There total 4 articles about 2,4-dinitrobenzylidene diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4-dinitrotoluene (121-14-2) + acetic anhydride (108-24-7) → 2,4-dinitrobenzyl acetate (29024-77-9) + 2,4-dinitrobenzylidene diacetate (1500090-76-5) + 2,4-dinitrobenzoic acid (610-30-0)

Guidance literature:

With sulfuric acid; manganese(II) acetate; ozone; at 20 ℃; Reagent/catalyst; Concentration; Temperature; Kinetics;

DOI:10.1134/S0023158413060050

Reference yield:

2,4-dinitrobenzyl alcohol (4836-66-2) → 2,4-dinitrobenzylidene diacetate (1500090-76-5)

Guidance literature:

Multi-step reaction with 2 steps

1: ozone; manganese(II) acetate; sulfuric acid / 20 °C / 760.05 Torr

2: ozone; manganese(II) acetate; sulfuric acid / 20 °C / 760.05 Torr

With sulfuric acid; manganese(II) acetate; ozone;

DOI:10.1134/S1070427214010042

Reference yield:

2,4-dinitrobenzaldehyde (528-75-6) + acetic anhydride (108-24-7) → 2,4-dinitrobenzylidene diacetate (1500090-76-5)

Guidance literature:

With sulfuric acid; manganese(II) acetate; ozone; at 20 ℃; under 760.051 Torr; Temperature; Kinetics;

DOI:10.1134/S1070427214010042

upstream raw materials:

2,4-dinitrotoluene

acetic anhydride

2,4-dinitrobenzaldehyde

2,4-dinitrobenzyl acetate

Downstream raw materials:

2,4-dinitrobenzoic acid