benzyl (S)-1-((1S,2R)-2-acetamido-4-oxocyclohexyl)-2-oxopyrrolidin-3-ylcarbamate

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Chemical Name:benzyl (S)-1-((1S,2R)-2-acetamido-4-oxocyclohexyl)-2-oxopyrrolidin-3-ylcarbamate
CAS No.:1004536-70-2
Molecular Formula:C₂₀H₂₅N₃O₅
Molecular Weight:387.436
Hs Code.:

Synonyms:benzyl (S)-1-((1S,2R)-2-acetamido-4-oxocyclohexyl)-2-oxopyrrolidin-3-ylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl (S)-1-((1S,2R)-2-acetamido-4-oxocyclohexyl)-2-oxopyrrolidin-3-ylcarbamate

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Technology Process of benzyl (S)-1-((1S,2R)-2-acetamido-4-oxocyclohexyl)-2-oxopyrrolidin-3-ylcarbamate

There total 1 articles about benzyl (S)-1-((1S,2R)-2-acetamido-4-oxocyclohexyl)-2-oxopyrrolidin-3-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1004536-68-8
benzyl ((S)-1-((1S,2R,4R)-2-acetamido-4-aminocyclohexyl)-2-oxopyrrolidin-3-yl)carbamate

: 1004536-70-2
benzyl (S)-1-((1S,2R)-2-acetamido-4-oxocyclohexyl)-2-oxopyrrolidin-3-ylcarbamate

Guidance literature:: With 3,5-di-tert-butyl-o-benzoquinone; In methanol; at 20 ℃; for 2h;

Reference yield: 78.0%

: 1004536-70-2
benzyl (S)-1-((1S,2R)-2-acetamido-4-oxocyclohexyl)-2-oxopyrrolidin-3-ylcarbamate

: 75-64-9
tert-butylamine

: 1004536-73-5
benzyl ((S)-1-((1S,2R,4R)-2-acetamido-4-(tert-butylamino)cyclohexyl)-2-oxopyrrolidin-3-yI)carbamate

Guidance literature:: benzyl (S)-1-((1S,2R)-2-acetamido-4-oxocyclohexyl)-2-oxopyrrolidin-3-ylcarbamate; tert-butylamine; titanium(IV)isopropoxide; titanium tetrachloride; In dichloromethane; at -50 - 20 ℃; for 2.16667h;

With dimethylsulfide borane complex; In dichloromethane; at 10 - 20 ℃; for 5h;

Reference yield: 78.0%

: 1004536-70-2
benzyl (S)-1-((1S,2R)-2-acetamido-4-oxocyclohexyl)-2-oxopyrrolidin-3-ylcarbamate

: 75-64-9
tert-butylamine

: 1004536-73-5
benzyl ((S)-1-((1S,2R,4R)-2-acetamido-4-(tert-butylamino)cyclohexyl)-2-oxopyrrolidin-3-yI)carbamate

: C₂₄H₃₆N₄O₄

Guidance literature:: benzyl (S)-1-((1S,2R)-2-acetamido-4-oxocyclohexyl)-2-oxopyrrolidin-3-ylcarbamate; tert-butylamine; In dichloromethane;

With titanium(IV) isopropylate; dimethylsulfide borane complex; titanium tetrachloride; In dichloromethane; at 20 ℃; for 16h; Reagent/catalyst; Catalytic behavior;
DOI:10.1021/acsmedchemlett.1c00082