Technology Process of C36H72O5Si2
There total 5 articles about C36H72O5Si2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 4 steps
1: toluene-4-sulfonic acid / 2 h / Heating
2: toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 24 h / 20 °C
3: 1H-imidazole / N,N-dimethyl-formamide / 12 h / 20 °C
4: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / 0 - 20 °C
With
1H-imidazole; lithium aluminium tetrahydride; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
2: Baeyer-Villiger oxidation;
DOI:10.1016/j.tetlet.2011.10.108
- Guidance literature:
-
Multi-step reaction with 5 steps
1: N-Bromosuccinimide; sodium hydrogencarbonate / water / 14 h / 20 - 85 °C
2: toluene-4-sulfonic acid / 2 h / Heating
3: toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 24 h / 20 °C
4: 1H-imidazole / N,N-dimethyl-formamide / 12 h / 20 °C
5: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / 0 - 20 °C
With
1H-imidazole; N-Bromosuccinimide; lithium aluminium tetrahydride; sodium hydrogencarbonate; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
3: Baeyer-Villiger oxidation;
DOI:10.1016/j.tetlet.2011.10.108
