2-(ω-hydroxyethylphenyl)-3-methoxyindenone

Base Information

Chemical Name:2-(ω-hydroxyethylphenyl)-3-methoxyindenone
CAS No.:136054-94-9
Molecular Formula:C₁₈H₁₆O₃
Molecular Weight:280.323
Hs Code.:

Synonyms:2-(ω-hydroxyethylphenyl)-3-methoxyindenone

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Chemical Property of 2-(ω-hydroxyethylphenyl)-3-methoxyindenone

Chemical Property:

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Technology Process of 2-(ω-hydroxyethylphenyl)-3-methoxyindenone

There total 8 articles about 2-(ω-hydroxyethylphenyl)-3-methoxyindenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 28272-96-0
2-vinylbenzaldehyde

: 136054-94-9
2-(ω-hydroxyethylphenyl)-3-methoxyindenone

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / sodium methoxide, ethyl propionate / methanol / 3 h / Heating

2: 98 percent / potassium carbonate / acetone / 1 h / Heating

3: 1.) 9-BBN, 2.) sodium acetate, hydrogen peroxide / 1.) THF, reflux, 5 h, 2.) RT, 2 h

With 9-borabicyclo[3.3.1]nonane dimer; dihydrogen peroxide; sodium methylate; sodium acetate; potassium carbonate; Ethyl propionate; In methanol; acetone;

Reference yield:

: 4122-56-9
methyl o-formylbenzoate

: 136054-94-9
2-(ω-hydroxyethylphenyl)-3-methoxyindenone

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) sodamide / 1.) ether, RT, 4 h, 2.) RT, 15 min

2: 95 percent / diisobutylaluminium hydride (DBAL-H, 20percent in hexane) / CH₂Cl₂ / 0.5 h / -78 °C

3: 95 percent / manganese dioxide / CH₂Cl₂ / 3 h / Ambient temperature

4: 70 percent / sodium methoxide, ethyl propionate / methanol / 3 h / Heating

5: 98 percent / potassium carbonate / acetone / 1 h / Heating

6: 1.) 9-BBN, 2.) sodium acetate, hydrogen peroxide / 1.) THF, reflux, 5 h, 2.) RT, 2 h

With manganese(IV) oxide; 9-borabicyclo[3.3.1]nonane dimer; dihydrogen peroxide; sodium methylate; sodium acetate; diisobutylaluminium hydride; potassium carbonate; sodium amide; Ethyl propionate; In methanol; dichloromethane; acetone;

Reference yield:

: 89-71-4
2-Methyl-benzoic acid methyl ester

: 136054-94-9
2-(ω-hydroxyethylphenyl)-3-methoxyindenone

Guidance literature:: Multi-step reaction with 8 steps

1: 95 percent / bromine, benzoyl peroxide / CCl₄ / 0.25 h / Heating; Irradiation

2: 82 percent / silver nitrate / tetrahydrofuran; H₂O / 0.5 h

3: 1.) sodamide / 1.) ether, RT, 4 h, 2.) RT, 15 min

4: 95 percent / diisobutylaluminium hydride (DBAL-H, 20percent in hexane) / CH₂Cl₂ / 0.5 h / -78 °C

5: 95 percent / manganese dioxide / CH₂Cl₂ / 3 h / Ambient temperature

6: 70 percent / sodium methoxide, ethyl propionate / methanol / 3 h / Heating

7: 98 percent / potassium carbonate / acetone / 1 h / Heating

8: 1.) 9-BBN, 2.) sodium acetate, hydrogen peroxide / 1.) THF, reflux, 5 h, 2.) RT, 2 h

With manganese(IV) oxide; 9-borabicyclo[3.3.1]nonane dimer; Perbenzoic acid; dihydrogen peroxide; bromine; sodium methylate; sodium acetate; diisobutylaluminium hydride; potassium carbonate; sodium amide; silver nitrate; Ethyl propionate; In tetrahydrofuran; methanol; tetrachloromethane; dichloromethane; water; acetone;