3-(2,6-bis(4-methoxyphenyl)piperidin-4-ylideneamino)-2-thioxoimidazolidin-4-one

Base Information

Chemical Name:3-(2,6-bis(4-methoxyphenyl)piperidin-4-ylideneamino)-2-thioxoimidazolidin-4-one
CAS No.:1276544-32-1
Molecular Formula:C₂₂H₂₄N₄O₃S
Molecular Weight:424.524
Hs Code.:

Synonyms:3-(2,6-bis(4-methoxyphenyl)piperidin-4-ylideneamino)-2-thioxoimidazolidin-4-one

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Chemical Property of 3-(2,6-bis(4-methoxyphenyl)piperidin-4-ylideneamino)-2-thioxoimidazolidin-4-one

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Technology Process of 3-(2,6-bis(4-methoxyphenyl)piperidin-4-ylideneamino)-2-thioxoimidazolidin-4-one

There total 4 articles about 3-(2,6-bis(4-methoxyphenyl)piperidin-4-ylideneamino)-2-thioxoimidazolidin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 199285-47-7
2,6-bis(4-methoxyphenyl)piperidin-4-one

: 79-19-6
thiosemicarbazide

: 105-39-5
chloroacetic acid ethyl ester

: 1276544-32-1
3-(2,6-bis(4-methoxyphenyl)piperidin-4-ylideneamino)-2-thioxoimidazolidin-4-one

Guidance literature:: With silica gel supported sodium hydrogen sulphate; for 0.05h; Microwave irradiation;
DOI:10.3109/14756361003691878

Reference yield: 72.0%

: 105-39-5
chloroacetic acid ethyl ester

: 597577-95-2
C₂₀H₂₄N₄O₂S

: 1276544-32-1
3-(2,6-bis(4-methoxyphenyl)piperidin-4-ylideneamino)-2-thioxoimidazolidin-4-one

Guidance literature:: With sodium acetate; In ethanol; for 4h; Reflux;
DOI:10.1016/j.bmcl.2009.11.074

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 1276544-32-1
3-(2,6-bis(4-methoxyphenyl)piperidin-4-ylideneamino)-2-thioxoimidazolidin-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium acetate / Heating

2: silica gel supported sodium hydrogen sulphate / 0.05 h / Microwave irradiation

With ammonium acetate;
DOI:10.3109/14756361003691878