N,N-Bis--acetophenon-hydrazon

Base Information

Chemical Name:N,N-Bis--acetophenon-hydrazon
CAS No.:21136-34-5
Molecular Formula:C₂₂H₂₀Cl₂N₂
Molecular Weight:383.32
Hs Code.:

N,N-Bis-<p-chlor-benzyl>-acetophenon-hydrazon

Synonyms:N,N-Bis--acetophenon-hydrazon

Suppliers and Price of N,N-Bis--acetophenon-hydrazon

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N,N-Bis--acetophenon-hydrazon

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N,N-Bis--acetophenon-hydrazon

There total 3 articles about N,N-Bis--acetophenon-hydrazon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104-83-6
1-Chloro-4-(chloromethyl)benzene

: 13466-30-3
(1-phenylethylidene)hydrazine

: 21136-34-5
N,N-Bis--acetophenon-hydrazon

Guidance literature:: (1-phenylethylidene)hydrazine; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.25h;

1-Chloro-4-(chloromethyl)benzene; In tetrahydrofuran; at 20 ℃; for 5h; Reflux;
DOI:10.1002/anie.201209618

Reference yield:

: 98-86-2
acetophenone

: 21136-34-5
N,N-Bis--acetophenon-hydrazon

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrazine hydrate / 4 h / Reflux

2.1: sodium hydride / tetrahydrofuran / 0.25 h / 0 °C

2.2: 5 h / 20 °C / Reflux

With sodium hydride; hydrazine hydrate; In tetrahydrofuran;
DOI:10.1002/anie.201209618

Reference yield:

: 21136-34-5
N,N-Bis--acetophenon-hydrazon

Guidance literature:: Acetophenonhydrazon, Kaliumamid (2 Val), fl. NH3, ueber entspr. N,N-Dikaliumsalz, 2) 2 Val p-Chlor-benzylchlorid, 3) NH4Cl;
DOI:10.1021/ja01028a020