2-cyclopropyl-3-hydroxy-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylpropanamide

Base Information

• Chemical Name: 2-cyclopropyl-3-hydroxy-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylpropanamide
• CAS No.: 1068601-80-8
• Molecular Formula: C₁₆H₂₃NO₃
• Molecular Weight: 277.364

Synonyms:2-cyclopropyl-3-hydroxy-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylpropanamide

Chemical Property of 2-cyclopropyl-3-hydroxy-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylpropanamide

Chemical Property:

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Technology Process of 2-cyclopropyl-3-hydroxy-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylpropanamide

There total 1 articles about 2-cyclopropyl-3-hydroxy-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylpropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 2-cyclopropyl-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylacetamide (1068601-77-3) → 2-cyclopropyl-3-hydroxy-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylpropanamide (1068601-80-8)

Guidance literature:

2-cyclopropyl-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylacetamide; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 - 0 ℃; for 1h; Inert atmosphere;

formaldehyd; In tetrahydrofuran; hexane; at 0 - 23 ℃; Inert atmosphere;

DOI:10.1021/ja806021y

Reference yield: 100.0%

2-cyclopropyl-3-hydroxy-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylpropanamide (1068601-80-8) + methanesulfonyl chloride (124-63-0) → C17H25NO5S (1068601-82-0)

Guidance literature:

With triethylamine; In dichloromethane; at -60 ℃; for 0.516667h; Inert atmosphere;

DOI:10.1021/ja806021y

upstream raw materials:

formaldehyd

2-cyclopropyl-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylacetamide

Downstream raw materials:

C₁₇H₂₅NO₅S

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