2-cyclopropyl-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylacetamide

Base Information

Chemical Name:2-cyclopropyl-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylacetamide
CAS No.:1068601-77-3
Molecular Formula:C₁₅H₂₁NO₂
Molecular Weight:247.337
Hs Code.:

Synonyms:2-cyclopropyl-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-cyclopropyl-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylacetamide

Chemical Property:

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Technology Process of 2-cyclopropyl-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylacetamide

There total 1 articles about 2-cyclopropyl-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54322-65-5
cyclopropylacetyl chloride

: 90-82-4,7009-81-6,90-83-5,6912-63-6
pseudoephedrine

: 1068601-77-3
2-cyclopropyl-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylacetamide

Guidance literature:: With triethylamine; In tetrahydrofuran; dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ja806021y

Reference yield: 95.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1068601-77-3
2-cyclopropyl-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylacetamide

: 1068601-80-8
2-cyclopropyl-3-hydroxy-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylpropanamide

Guidance literature:: 2-cyclopropyl-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylacetamide; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 - 0 ℃; for 1h; Inert atmosphere;

formaldehyd; In tetrahydrofuran; hexane; at 0 - 23 ℃; Inert atmosphere;
DOI:10.1021/ja806021y

Reference yield: 88.0%

: 1068601-77-3
2-cyclopropyl-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylacetamide

: 1251530-48-9
C₁₀H₁₂ClIO

: 1251530-49-0
C₂₅H₃₂ClNO₃

Guidance literature:: 2-cyclopropyl-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylacetamide; With lithium chloride; lithium diisopropyl amide; In tetrahydrofuran; at -78 - 0 ℃; for 1.5h;

C₁₀H₁₂ClIO; In tetrahydrofuran; at 0 - 20 ℃; for 20h;
DOI:10.1016/j.bmcl.2010.07.030