C₃₀H₂₉NO₇

Base Information

Chemical Name:C₃₀H₂₉NO₇
CAS No.:288395-79-9
Molecular Formula:C₃₀H₂₉NO₇
Molecular Weight:515.563
Hs Code.:

C<sub>30</sub>H<sub>29</sub>NO<sub>7</sub>

Synonyms:C₃₀H₂₉NO₇

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Chemical Property of C₃₀H₂₉NO₇

Chemical Property:

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Technology Process of C₃₀H₂₉NO₇

There total 21 articles about C₃₀H₂₉NO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: C₂₃H₂₃NO₇

: 288395-79-9
C₃₀H₂₉NO₇

Guidance literature:: C₂₃H₂₃NO₇; With sodium hydride; In N,N-dimethyl-formamide; at -20 ℃; for 0.5h;

benzyl bromide; tetra-(n-butyl)ammonium iodide; In N,N-dimethyl-formamide; at -10 ℃; for 1h; Further stages.;
DOI:10.1021/ja000930i

Reference yield:

: 7797-83-3
2H-benzo[d]1,3-dioxolane-4-carbaldehyde

: 288395-79-9
C₃₀H₂₉NO₇

Guidance literature:: Multi-step reaction with 12 steps

1.1: aq. m-chloroperbenzoic acid / CH₂Cl₂ / 24 h / Heating

1.2: 63 percent / KOH / ethanol / 2 h / 20 °C

2.1: 90 percent / silver trifluoroacetate; Br₂ / CHCl₃ / 1 h / 10 - 15 °C

3.1: 94 percent / pyridinium p-toluenesulfonate / CH₂Cl₂ / 2 h

4.1: n-BuLi / tetrahydrofuran; pentane / 0.5 h / -100 °C

4.2: tetrahydrofuran; toluene; pentane / 0.75 h / -100 °C

5.1: NaH / dimethylformamide / 0.5 h / -5 °C

5.2: dimethylformamide / 0.25 h / -5 °C

6.1: 76 percent / pyridinium p-toluenesulfonate / methanol / 2 h / 20 °C

7.1: 30 percent / benzene / 48 h / 5 °C / UV-irradiation

8.1: NaH / tetrahydrofuran / 0.5 h / 0 °C

8.2: 98 percent / tetrahydrofuran / 24 h / 20 °C

9.1: 85 percent / tetrabutylammonium fluoride / tetrahydrofuran / 0.33 h / -5 °C

10.1: 83 percent / Dess-Martin periodinane / CH₂Cl₂ / 4 h

11.1: NaBH₄ / methanol / 0.5 h / -20 °C

12.1: NaH / dimethylformamide / 0.5 h / -20 °C

12.2: 47 mg / tetrabutylammonium iodide / dimethylformamide / 1 h / -10 °C

With sodium tetrahydroborate; n-butyllithium; tetrabutyl ammonium fluoride; bromine; silver trifluoroacetate; pyridinium p-toluenesulfonate; sodium hydride; Dess-Martin periodane; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane; chloroform; N,N-dimethyl-formamide; pentane; benzene; 1.1: Rearrangement / 1.2: Hydrolysis / 2.1: Bromination / 3.1: Addition / 4.1: Metallation / 4.2: Addition / 5.1: Metallation / 5.2: Substitution / 6.1: deprotection / 7.1: Cyclization / 8.1: Metallation / 8.2: Methylation / 9.1: Hydrolysis / 10.1: Oxidation / 11.1: Reduction / 12.1: Metallation / 12.2: Alkylation;
DOI:10.1021/ja000930i

Reference yield:

: 6493-77-2
methyl cyclohex-3-ene-1-carboxylate

: 288395-79-9
C₃₀H₂₉NO₇

Guidance literature:: Multi-step reaction with 16 steps

1.1: N-bromosuccinimide; azobis(isobutyronitrile) / benzene / 0.33 h / Heating

1.2: tri-n-butyltinhydride; azobis(isobutyronitrile) / benzene / 3.5 h / Heating

2.1: O₂; Rose Bengal / acetone / 8 h / -10 °C / Irradiation

2.2: RuCl₂(PPh₃)3 / CH₂Cl₂ / -10 - 20 °C

2.3: 42 percent / NaOMe / methanol / 0.5 h / -5 °C

3.1: 99 percent / Et₃N; 4-dimethylaminopyridine / CH₂Cl₂ / 0 - 20 °C

4.1: 80 percent Turnov_. / cholesterol esterase; aq. NaOH / 36 h / 5 °C / pH 7.7

5.1: 98 percent / imidazole / dimethylformamide / 0.67 h / 20 °C

6.1: 81 percent Turnov_. / LiOH*H₂O / methanol / 48 h / -5 °C

7.1: diphenylphosphorazidate; Et₃N / benzene / 1 h

7.2: toluene / 1 h / 110 °C

8.1: n-BuLi / tetrahydrofuran; pentane / 0.5 h / -100 °C

8.2: tetrahydrofuran; toluene; pentane / 0.75 h / -100 °C

9.1: NaH / dimethylformamide / 0.5 h / -5 °C

9.2: dimethylformamide / 0.25 h / -5 °C

10.1: 76 percent / pyridinium p-toluenesulfonate / methanol / 2 h / 20 °C

11.1: 30 percent / benzene / 48 h / 5 °C / UV-irradiation

12.1: NaH / tetrahydrofuran / 0.5 h / 0 °C

12.2: 98 percent / tetrahydrofuran / 24 h / 20 °C

13.1: 85 percent / tetrabutylammonium fluoride / tetrahydrofuran / 0.33 h / -5 °C

14.1: 83 percent / Dess-Martin periodinane / CH₂Cl₂ / 4 h

15.1: NaBH₄ / methanol / 0.5 h / -20 °C

16.1: NaH / dimethylformamide / 0.5 h / -20 °C

16.2: 47 mg / tetrabutylammonium iodide / dimethylformamide / 1 h / -10 °C

With 1H-imidazole; dmap; lithium hydroxide; sodium hydroxide; sodium tetrahydroborate; N-Bromosuccinimide; n-butyllithium; cholesterol esterase; 2,2'-azobis(isobutyronitrile); diphenyl phosphoryl azide; tetrabutyl ammonium fluoride; oxygen; pyridinium p-toluenesulfonate; rose bengal; sodium hydride; Dess-Martin periodane; triethylamine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetone; pentane; benzene; 1.1: Bromination / 1.2: Dehydrobromination / 2.1: Oxidation / 2.2: Epoxidation / 2.3: Ring cleavage / 3.1: Acylation / 4.1: Hydrolysis / 5.1: silylation / 6.1: Hydrolysis / 7.1: azidation / 7.2: Rearrangement / 8.1: Metallation / 8.2: Addition / 9.1: Metallation / 9.2: Substitution / 10.1: deprotection / 11.1: Cyclization / 12.1: Metallation / 12.2: Methylation / 13.1: Hydrolysis / 14.1: Oxidation / 15.1: Reduction / 16.1: Metallation / 16.2: Alkylation;
DOI:10.1021/ja000930i