cis-8-azido-6-(tert-butyl-diphenyl-silanyloxymethyl)-8-phenyl-5,6-dihydro-8H-tetrazolo[5,1-c][1,4]oxazine

Base Information

Chemical Name:cis-8-azido-6-(tert-butyl-diphenyl-silanyloxymethyl)-8-phenyl-5,6-dihydro-8H-tetrazolo[5,1-c][1,4]oxazine
CAS No.:1187063-50-8
Molecular Formula:C₂₇H₂₉N₇O₂Si
Molecular Weight:511.658
Hs Code.:

Synonyms:cis-8-azido-6-(tert-butyl-diphenyl-silanyloxymethyl)-8-phenyl-5,6-dihydro-8H-tetrazolo[5,1-c][1,4]oxazine

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Chemical Property of cis-8-azido-6-(tert-butyl-diphenyl-silanyloxymethyl)-8-phenyl-5,6-dihydro-8H-tetrazolo[5,1-c][1,4]oxazine

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Technology Process of cis-8-azido-6-(tert-butyl-diphenyl-silanyloxymethyl)-8-phenyl-5,6-dihydro-8H-tetrazolo[5,1-c][1,4]oxazine

There total 1 articles about cis-8-azido-6-(tert-butyl-diphenyl-silanyloxymethyl)-8-phenyl-5,6-dihydro-8H-tetrazolo[5,1-c][1,4]oxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 1187063-28-0
cis-6-(tert-butyl-diphenyl-silanyloxymethyl)-8-phenyl-5,6-dihydro-8H-tetrazolo[5,1-c][1,4]oxazine

: 1187063-52-0
[6-(tert-butyl-diphenyl-silanyloxymethyl)-5,6-dihydro-tetrazolo-[5,1-c][1,4]oxazin-8-ylidene]-phenyl-amine

: 1187063-50-8
cis-8-azido-6-(tert-butyl-diphenyl-silanyloxymethyl)-8-phenyl-5,6-dihydro-8H-tetrazolo[5,1-c][1,4]oxazine

: 8-azido-6-(tert-butyl-diphenyl-silanyloxymethyl)-8-phenyl-5,6-dihydro-8H-tetrazolo[5,1-c][1,4]oxazine

Guidance literature:: With iodine(I) azide; In acetonitrile; for 36h; optical yield given as %de; Reflux;
DOI:10.1016/j.tet.2009.06.033

Reference yield: 79.0%

: 1187063-50-8
cis-8-azido-6-(tert-butyl-diphenyl-silanyloxymethyl)-8-phenyl-5,6-dihydro-8H-tetrazolo[5,1-c][1,4]oxazine

: 108-24-7
acetic anhydride

: 1187063-69-9
acetic acid 2-(5-benzoyl-tetrazol-1-yl)-1-(tert-butyldiphenyl-silanyloxymethyl)-ethyl ester

Guidance literature:: cis-8-azido-6-(tert-butyl-diphenyl-silanyloxymethyl)-8-phenyl-5,6-dihydro-8H-tetrazolo[5,1-c][1,4]oxazine; With trimethylphosphane; In tetrahydrofuran; at 50 ℃; for 0.5h;

With ammonium hydroxide; In tetrahydrofuran; water; at 20 - 35 ℃; for 2h;

acetic anhydride; With pyridine; at 0 - 20 ℃; for 8h;
DOI:10.1016/j.tet.2009.06.033