2-{Benzenesulfonyl-[2-(2-formyl-pyrrol-1-ylmethyl)-allyl]-amino}-benzoic acid methyl ester

Base Information

• Chemical Name: 2-{Benzenesulfonyl-[2-(2-formyl-pyrrol-1-ylmethyl)-allyl]-amino}-benzoic acid methyl ester
• CAS No.: 145984-02-7
• Molecular Formula: C₂₃H₂₂N₂O₅S
• Molecular Weight: 438.504

Synonyms:2-{Benzenesulfonyl-[2-(2-formyl-pyrrol-1-ylmethyl)-allyl]-amino}-benzoic acid methyl ester

Chemical Property of 2-{Benzenesulfonyl-[2-(2-formyl-pyrrol-1-ylmethyl)-allyl]-amino}-benzoic acid methyl ester

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Technology Process of 2-{Benzenesulfonyl-[2-(2-formyl-pyrrol-1-ylmethyl)-allyl]-amino}-benzoic acid methyl ester

There total 3 articles about 2-{Benzenesulfonyl-[2-(2-formyl-pyrrol-1-ylmethyl)-allyl]-amino}-benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-[2-(2-Formyl-pyrrol-1-ylmethyl)-allyl]-N-(2-iodo-phenyl)-benzenesulfonamide (145984-00-5) → C21H18N2O3S (145984-03-8) + 2-{Benzenesulfonyl-[2-(2-formyl-pyrrol-1-ylmethyl)-allyl]-amino}-benzoic acid methyl ester (145984-02-7) + [1-Benzenesulfonyl-3-(2-formyl-pyrrol-1-ylmethyl)-2,3-dihydro-1H-indol-3-yl]-acetic acid methyl ester (145984-01-6)

Guidance literature:

With carbon monoxide; thallium(I) acetate; bis-triphenylphosphine-palladium(II) chloride; In methanol; at 65 ℃; for 21h; under 760 Torr; Yield given. Yields of byproduct given;

DOI:10.1016/0040-4039(93)88047-M

Reference yield:

methanol (67-56-1) + carbon monoxide (201230-82-2) + N-[2-(2-Formyl-pyrrol-1-ylmethyl)-allyl]-N-(2-iodo-phenyl)-benzenesulfonamide (145984-00-5) → 2-{Benzenesulfonyl-[2-(2-formyl-pyrrol-1-ylmethyl)-allyl]-amino}-benzoic acid methyl ester (145984-02-7) + [1-Benzenesulfonyl-3-(2-formyl-pyrrol-1-ylmethyl)-2,3-dihydro-1H-indol-3-yl]-acetic acid methyl ester (145984-01-6)

Guidance literature:

With triethylamine; bis-triphenylphosphine-palladium(II) chloride; at 65 ℃; for 21h; under 6205.8 Torr; Yield given. Yields of byproduct given;

DOI:10.1016/0040-4039(93)88047-M

Reference yield:

methanol (67-56-1) + carbon monoxide (201230-82-2) + N-[2-(2-Formyl-pyrrol-1-ylmethyl)-allyl]-N-(2-iodo-phenyl)-benzenesulfonamide (145984-00-5) → C21H18N2O3S (145984-03-8) + 2-{Benzenesulfonyl-[2-(2-formyl-pyrrol-1-ylmethyl)-allyl]-amino}-benzoic acid methyl ester (145984-02-7) + [1-Benzenesulfonyl-3-(2-formyl-pyrrol-1-ylmethyl)-2,3-dihydro-1H-indol-3-yl]-acetic acid methyl ester (145984-01-6)

Guidance literature:

With thallium(I) acetate; bis-triphenylphosphine-palladium(II) chloride; at 65 ℃; for 21h; under 760 Torr; Yield given. Yields of byproduct given;

DOI:10.1016/0040-4039(93)88047-M

upstream raw materials:

methanol

carbon monoxide

N-[2-(2-Formyl-pyrrol-1-ylmethyl)-allyl]-N-(2-iodo-phenyl)-benzenesulfonamide

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