cycloheptyl phenyl sulfide

Base Information

• Chemical Name: cycloheptyl phenyl sulfide
• CAS No.: 10181-76-7
• Molecular Formula: C₁₃H₁₈S
• Molecular Weight: 206.352
• Mol file: 10181-76-7.mol

Synonyms:cycloheptyl phenyl sulfide

Chemical Property of cycloheptyl phenyl sulfide

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of cycloheptyl phenyl sulfide

There total 5 articles about cycloheptyl phenyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

sodium S-cycloheptyl sulfothioate (1561023-29-7) + phenylmagnesium bromide (100-58-3) → cycloheptyl phenyl sulfide (10181-76-7)

Guidance literature:

In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere; Green chemistry;

DOI:10.1021/ol500067f

Reference yield: 80.0%

cycloheptyl bromide (2404-35-5) + sodium thiophenolate (930-69-8) → cycloheptyl phenyl sulfide (10181-76-7)

Guidance literature:

In acetonitrile;

DOI:10.1002/1099-1395(200102)14:2<81::AID-POC338>3.0.CO;2-Z

Reference yield: 61.0%

methyl benzenesulfinate (670-98-4) + cycloheptane (291-64-5) → cycloheptyl phenyl sulfide (10181-76-7)

Guidance literature:

With di-tert-butyl peroxide; iodine; phosphonic acid diethyl ester; In acetonitrile; at 140 ℃; for 24h; Sealed tube;

DOI:10.1002/asia.201601376

upstream raw materials:

Cycloheptene

thiophenol

cycloheptyl bromide

sodium thiophenolate

Downstream raw materials:

1-(1-cycloheptenyl)-4-methylbenzene

phenyl cycloheptyl sulfoxide