ethyl 3-(1,3-dibenzyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-5-yl)-3,3-ethylenedioxypropionate

Base Information

Chemical Name:ethyl 3-(1,3-dibenzyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-5-yl)-3,3-ethylenedioxypropionate
CAS No.:934365-25-0
Molecular Formula:C₂₅H₂₆N₂O₆
Molecular Weight:450.491
Hs Code.:

Synonyms:ethyl 3-(1,3-dibenzyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-5-yl)-3,3-ethylenedioxypropionate

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Chemical Property of ethyl 3-(1,3-dibenzyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-5-yl)-3,3-ethylenedioxypropionate

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Technology Process of ethyl 3-(1,3-dibenzyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-5-yl)-3,3-ethylenedioxypropionate

There total 4 articles about ethyl 3-(1,3-dibenzyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-5-yl)-3,3-ethylenedioxypropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 934365-24-9
C₂₃H₂₂N₂O₅

: 107-21-1
ethylene glycol

: 934365-25-0
ethyl 3-(1,3-dibenzyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-5-yl)-3,3-ethylenedioxypropionate

Guidance literature:: With orthoformic acid triethyl ester; pyridinium p-toluenesulfonate;
DOI:10.1016/j.bmcl.2006.12.009

Reference yield:

: 57667-73-9
N,N'-dibenzyluracil-5-carbaldehyde

: 934365-25-0
ethyl 3-(1,3-dibenzyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-5-yl)-3,3-ethylenedioxypropionate

Guidance literature:: Multi-step reaction with 2 steps

1: tin(II) chloride / CH₂Cl₂

2: CH(OEt)3 / PTS

With orthoformic acid triethyl ester; tin(ll) chloride; pyridinium p-toluenesulfonate; In dichloromethane;
DOI:10.1016/j.bmcl.2006.12.009

Reference yield:

: 1195-08-0
2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde

: 934365-25-0
ethyl 3-(1,3-dibenzyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-5-yl)-3,3-ethylenedioxypropionate

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / K₂CO₃ / dimethylformamide

2: tin(II) chloride / CH₂Cl₂

3: CH(OEt)3 / PTS

With potassium carbonate; orthoformic acid triethyl ester; tin(ll) chloride; pyridinium p-toluenesulfonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2006.12.009