7-(2-((tert-butyldimethylsilyl)oxy)ethoxy)-2-(4-nitrophenyl)-quinoxaline

Base Information Edit

Chemical Name:7-(2-((tert-butyldimethylsilyl)oxy)ethoxy)-2-(4-nitrophenyl)-quinoxaline
CAS No.:1437281-24-7
Molecular Formula:C₂₂H₂₇N₃O₄Si
Molecular Weight:425.56
Hs Code.:
Mol file:1437281-24-7.mol

Synonyms:7-(2-((tert-butyldimethylsilyl)oxy)ethoxy)-2-(4-nitrophenyl)-quinoxaline

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Chemical Property of 7-(2-((tert-butyldimethylsilyl)oxy)ethoxy)-2-(4-nitrophenyl)-quinoxaline Edit

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Technology Process of 7-(2-((tert-butyldimethylsilyl)oxy)ethoxy)-2-(4-nitrophenyl)-quinoxaline

There total 2 articles about 7-(2-((tert-butyldimethylsilyl)oxy)ethoxy)-2-(4-nitrophenyl)-quinoxaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.3%

: 1437281-18-9
3-(4-nitrophenyl)quinoxalin-6-ol

: 86864-60-0
2-(tert-butyldimethylsilyloxy)ethyl bromide

: 1437281-24-7
7-(2-((tert-butyldimethylsilyl)oxy)ethoxy)-2-(4-nitrophenyl)-quinoxaline

Guidance literature:: 3-(4-nitrophenyl)quinoxalin-6-ol; With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 1h;

2-(tert-butyldimethylsilyloxy)ethyl bromide; In N,N-dimethyl-formamide; at 80 ℃;
DOI:10.1021/ml4000707

Reference yield:

: 1437281-17-8
7-((tert-butyldimethylsilyl)oxy)-2-(4-nitrophenyl)quinoxaline

: 1437281-24-7
7-(2-((tert-butyldimethylsilyl)oxy)ethoxy)-2-(4-nitrophenyl)-quinoxaline

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 - 20 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 80 °C

2.2: 80 °C

With tetrabutyl ammonium fluoride; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;