p-nitrophenyl 4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranoside

Base Information

Chemical Name:p-nitrophenyl 4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranoside
CAS No.:14675-51-5
Molecular Formula:C₁₆H₁₇NO₈
Molecular Weight:351.313
Hs Code.:

Synonyms:p-nitrophenyl 4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranoside

Suppliers and Price of p-nitrophenyl 4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-nitrophenyl 4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranoside

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Technology Process of p-nitrophenyl 4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranoside

There total 4 articles about p-nitrophenyl 4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 2873-29-2
D-glucal triacetate

: 14675-51-5,56196-13-5
p-nitrophenyl 4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranoside

Guidance literature:: With zinc dibromide; In chloroform; at 72 ℃; for 0.75h; stereoselective reaction; Microwave irradiation;
DOI:10.1080/00397911.2014.909490

Reference yield: 40.0%

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 2873-29-2
D-glucal triacetate

: 14675-51-5,56196-13-5
p-nitrophenyl 4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranoside

: 14675-52-6,56196-13-5
p-nitrophenyl 4,6-di-O-acetyl-2,3-dideoxy-β-D-erythro-hex-2-enopyranoside

Guidance literature:: In chlorobenzene; for 15h; Heating;
DOI:10.1080/00397919508011424

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 118356-98-2
4,6-di-O-acetyl-3-O-D-glucal

: 14675-51-5,56196-13-5
p-nitrophenyl 4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranoside

: 14675-52-6,56196-13-5
p-nitrophenyl 4,6-di-O-acetyl-2,3-dideoxy-β-D-erythro-hex-2-enopyranoside

Guidance literature:: With azodicarboxylic acid bis(2-methoxyethyl) ester; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 24h; optical yield given as %de; stereoselective reaction;
DOI:10.1016/j.tet.2011.11.084