phenyl N-[1-(4-phenoxyphenoxy)-3-(2H-tetrazol-2-yl)propan-2-yl]carbamate

Base Information

Chemical Name:phenyl N-[1-(4-phenoxyphenoxy)-3-(2H-tetrazol-2-yl)propan-2-yl]carbamate
CAS No.:1610891-36-5
Molecular Formula:C₂₃H₂₁N₅O₄
Molecular Weight:431.451
Hs Code.:

Synonyms:phenyl N-[1-(4-phenoxyphenoxy)-3-(2H-tetrazol-2-yl)propan-2-yl]carbamate

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Chemical Property of phenyl N-[1-(4-phenoxyphenoxy)-3-(2H-tetrazol-2-yl)propan-2-yl]carbamate

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Technology Process of phenyl N-[1-(4-phenoxyphenoxy)-3-(2H-tetrazol-2-yl)propan-2-yl]carbamate

There total 5 articles about phenyl N-[1-(4-phenoxyphenoxy)-3-(2H-tetrazol-2-yl)propan-2-yl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1610891-34-3
1-(4-phenoxyphenoxy)-3-(2H-tetrazol-2-yl)propan-2-amine hydrochloride

: 1885-14-9
phenyl chloroformate

: 1610891-36-5
phenyl N-[1-(4-phenoxyphenoxy)-3-(2H-tetrazol-2-yl)propan-2-yl]carbamate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 2h;
DOI:10.1080/00397911.2013.868490

Reference yield:

: 1610891-25-2
tert-butyl N-[2-hydroxy-3-(4-phenoxyphenoxy)propyl]carbamate

: 1610891-36-5
phenyl N-[1-(4-phenoxyphenoxy)-3-(2H-tetrazol-2-yl)propan-2-yl]carbamate

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine; dmap / dichloromethane / 12 h / 20 °C

2: tetra(n-butyl)ammonium hydrogensulfate; potassium hydroxide / dichloromethane / 12 h / 20 °C

3: boron trifluoride diethyl etherate / acetonitrile; dichloromethane / 3 h / 20 °C

4: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

5: triethylamine / tetrahydrofuran / 2 h / 0 - 20 °C

With dmap; boron trifluoride diethyl etherate; tetra(n-butyl)ammonium hydrogensulfate; triethylamine; trifluoroacetic acid; potassium hydroxide; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1080/00397911.2013.868490

Reference yield:

: 1610891-26-3
1-[(tert-butoxycarbonyl)amino]-3-(4-phenoxyphenoxy)propan-2-yl 4-methylbenzenesulfonate

: 1610891-36-5
phenyl N-[1-(4-phenoxyphenoxy)-3-(2H-tetrazol-2-yl)propan-2-yl]carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: tetra(n-butyl)ammonium hydrogensulfate; potassium hydroxide / dichloromethane / 12 h / 20 °C

2: boron trifluoride diethyl etherate / acetonitrile; dichloromethane / 3 h / 20 °C

3: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

4: triethylamine / tetrahydrofuran / 2 h / 0 - 20 °C

With boron trifluoride diethyl etherate; tetra(n-butyl)ammonium hydrogensulfate; triethylamine; trifluoroacetic acid; potassium hydroxide; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1080/00397911.2013.868490