3,3-Bis-ethylsulfanyl-2-(2,4,5-trifluoro-benzoyl)-acrylic acid ethyl ester

Base Information

Chemical Name:3,3-Bis-ethylsulfanyl-2-(2,4,5-trifluoro-benzoyl)-acrylic acid ethyl ester
CAS No.:154359-92-9
Molecular Formula:C₁₆H₁₇F₃O₃S₂
Molecular Weight:378.436
Hs Code.:

Synonyms:3,3-Bis-ethylsulfanyl-2-(2,4,5-trifluoro-benzoyl)-acrylic acid ethyl ester

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Chemical Property of 3,3-Bis-ethylsulfanyl-2-(2,4,5-trifluoro-benzoyl)-acrylic acid ethyl ester

Chemical Property:

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Technology Process of 3,3-Bis-ethylsulfanyl-2-(2,4,5-trifluoro-benzoyl)-acrylic acid ethyl ester

There total 1 articles about 3,3-Bis-ethylsulfanyl-2-(2,4,5-trifluoro-benzoyl)-acrylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-15-0,12122-00-8
carbon disulfide

: 98349-24-7
ethyl 2,4,5-trifluorobenzoylacetate

: 75-03-6
ethyl iodide

: 154359-92-9
3,3-Bis-ethylsulfanyl-2-(2,4,5-trifluoro-benzoyl)-acrylic acid ethyl ester

Guidance literature:: With potassium carbonate; Yield given. Multistep reaction; 1.) DMF, 0 deg C, 5 min, 2.) DMF, 0 deg C, 3 h;
DOI:10.1002/jhet.5570340622

Reference yield: 53.0%

: 154359-92-9
3,3-Bis-ethylsulfanyl-2-(2,4,5-trifluoro-benzoyl)-acrylic acid ethyl ester

: (Z)-3-Amino-3-ethylsulfanyl-2-(2,4,5-trifluoro-benzoyl)-acrylic acid ethyl ester

Guidance literature:: With ammonia; In ethanol; at 80 ℃; for 18h;
DOI:10.1002/jhet.5570340622

Reference yield:

: 154359-92-9
3,3-Bis-ethylsulfanyl-2-(2,4,5-trifluoro-benzoyl)-acrylic acid ethyl ester

: 849744-52-1,154330-67-3
ethyl 4-hydroxy-6,7-difluoro-2-(ethylthio)quinoline-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 53 percent / NH₃ / ethanol / 18 h / 80 °C

2: 58 percent / KHCO₃ / dimethylformamide / 24 h / 80 °C

With ammonia; potassium hydrogencarbonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570340622