Technology Process of BOCCys(Bzl)TyrIleOMe
There total 4 articles about BOCCys(Bzl)TyrIleOMe which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
TEA; carbonochloridic acid, butyl ester;
In
diethyl ether;
1) -10 deg C, 30 min, 2) 0 deg C, 18 h;
DOI:10.1007/BF00596712
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 87 percent / N-hydroxysuccinimide (HOSu), dicyclohexylcarbodiimid (DCHC) / various solvent(s) / 0 °C
2: 87 percent / hydrogen / palladium black / methanol / 20 h / Ambient temperature
3: 92 percent / butyl chloroformate, TEA / diethyl ether / 1) -10 deg C, 30 min, 2) 0 deg C, 18 h
With
1-hydroxy-pyrrolidine-2,5-dione; TEA; hydrogen; carbonochloridic acid, butyl ester; dicyclohexyl-carbodiimide;
palladium;
In
methanol; diethyl ether;
DOI:10.1007/BF00596712
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 87 percent / N-hydroxysuccinimide (HOSu), dicyclohexylcarbodiimid (DCHC) / various solvent(s) / 0 °C
2: 87 percent / hydrogen / palladium black / methanol / 20 h / Ambient temperature
3: 92 percent / butyl chloroformate, TEA / diethyl ether / 1) -10 deg C, 30 min, 2) 0 deg C, 18 h
With
1-hydroxy-pyrrolidine-2,5-dione; TEA; hydrogen; carbonochloridic acid, butyl ester; dicyclohexyl-carbodiimide;
palladium;
In
methanol; diethyl ether;
DOI:10.1007/BF00596712
