1,6-anhydro-4-O-benzyl-2,3-dideoxy-β-D-allopyrano<2,3-d>-2-methoxy-2-thiazoline

Base Information

Chemical Name:1,6-anhydro-4-O-benzyl-2,3-dideoxy-β-D-allopyrano<2,3-d>-2-methoxy-2-thiazoline
CAS No.:101024-18-4
Molecular Formula:C₁₅H₁₇NO₄S
Molecular Weight:307.37
Hs Code.:

Synonyms:1,6-anhydro-4-O-benzyl-2,3-dideoxy-β-D-allopyrano<2,3-d>-2-methoxy-2-thiazoline

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Chemical Property of 1,6-anhydro-4-O-benzyl-2,3-dideoxy-β-D-allopyrano<2,3-d>-2-methoxy-2-thiazoline

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Technology Process of 1,6-anhydro-4-O-benzyl-2,3-dideoxy-β-D-allopyrano<2,3-d>-2-methoxy-2-thiazoline

There total 4 articles about 1,6-anhydro-4-O-benzyl-2,3-dideoxy-β-D-allopyrano<2,3-d>-2-methoxy-2-thiazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 67-56-1
methanol

: 101024-14-0
1,6-anhydro-4-O-benzyl-2-deoxy-2-isothiocyanato-3-O-p-toluenesulfonyl-β-D-glucopyranose

: 101024-18-4
1,6-anhydro-4-O-benzyl-2,3-dideoxy-β-D-allopyrano<2,3-d>-2-methoxy-2-thiazoline

Guidance literature:: With triethylamine; at 80 ℃; for 4h; high pressure;

Reference yield:

: 50447-92-2
2-amino-1,6-anhydro-4-O-benzyl-2-deoxy-β-D-glucopyranose

: 101024-18-4
1,6-anhydro-4-O-benzyl-2,3-dideoxy-β-D-allopyrano<2,3-d>-2-methoxy-2-thiazoline

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydrogen carbonate / dioxane; H₂O

2: NaOH, I₂ / dioxane; aq. ethanol

3: 77 percent / pyridine / 4 h / Heating

4: 90 percent / triethylamine / 4 h / 80 °C / high pressure

With pyridine; sodium hydroxide; iodine; sodium hydrogencarbonate; triethylamine; In 1,4-dioxane; ethanol; water;

Reference yield:

: 101024-10-6
C₁₄H₁₆NO₄S₂^(1-)*Na⁽¹⁺⁾

: 101024-18-4
1,6-anhydro-4-O-benzyl-2,3-dideoxy-β-D-allopyrano<2,3-d>-2-methoxy-2-thiazoline

Guidance literature:: Multi-step reaction with 3 steps

1: NaOH, I₂ / dioxane; aq. ethanol

2: 77 percent / pyridine / 4 h / Heating

3: 90 percent / triethylamine / 4 h / 80 °C / high pressure

With pyridine; sodium hydroxide; iodine; triethylamine; In 1,4-dioxane; ethanol;