acetic acid 3-(4-methoxyphenyl)-2-(4-methoxyphenylazo)-2-methylpropyl ester

Base Information

Chemical Name:acetic acid 3-(4-methoxyphenyl)-2-(4-methoxyphenylazo)-2-methylpropyl ester
CAS No.:927196-12-1
Molecular Formula:C₂₀H₂₄N₂O₄
Molecular Weight:356.422
Hs Code.:

Synonyms:acetic acid 3-(4-methoxyphenyl)-2-(4-methoxyphenylazo)-2-methylpropyl ester

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Chemical Property of acetic acid 3-(4-methoxyphenyl)-2-(4-methoxyphenylazo)-2-methylpropyl ester

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Technology Process of acetic acid 3-(4-methoxyphenyl)-2-(4-methoxyphenylazo)-2-methylpropyl ester

There total 1 articles about acetic acid 3-(4-methoxyphenyl)-2-(4-methoxyphenylazo)-2-methylpropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 820-71-3
methallyl acetate

: 459-64-3
4-methoxybenzenediazonium tetrafluoroborate

: 927196-12-1
acetic acid 3-(4-methoxyphenyl)-2-(4-methoxyphenylazo)-2-methylpropyl ester

Guidance literature:: With ferrous(II) sulfate heptahydrate; In water; dimethyl sulfoxide; at 20 ℃; for 0.333333h; Inert atmosphere;
DOI:10.1002/ejoc.200800250

Reference yield:

: 927196-12-1
acetic acid 3-(4-methoxyphenyl)-2-(4-methoxyphenylazo)-2-methylpropyl ester

: C₁₁H₁₇NO₂

: 1268388-02-8
C₁₁H₁₇NO₂

Guidance literature:: acetic acid 3-(4-methoxyphenyl)-2-(4-methoxyphenylazo)-2-methylpropyl ester; In tert-butyl methyl ether; at 40 ℃; for 168h; pH=7.5; Enzymatic reaction;

With hydrogenchloride; zinc; In methanol; water; at 20 ℃; for 4h; enantioselective reaction;
DOI:10.1016/j.tetlet.2010.11.137

Reference yield:

: 927196-12-1
acetic acid 3-(4-methoxyphenyl)-2-(4-methoxyphenylazo)-2-methylpropyl ester

: 65555-88-6
α-methyl-β-p-methoxyphenyl-alanine

: 132616-92-3
O,α-dimethyl-D-tyrosine

Guidance literature:: acetic acid 3-(4-methoxyphenyl)-2-(4-methoxyphenylazo)-2-methylpropyl ester; In tert-butyl methyl ether; at 40 ℃; for 168h; pH=7.5; Enzymatic reaction;

With hydrogenchloride; water; zinc; In methanol; at 20 ℃; for 4h;

With sodium periodate; sodium dichromate; sulfuric acid; In water; at 20 ℃; for 20h; enantioselective reaction;
DOI:10.1016/j.tetlet.2010.11.137