tert-butyl {1-[4-(5,7-diethyl-3-phenylpyrazolo[1,5-a]pyrimidin-2-yl)phenyl]cyclobutyl}carbamate

Base Information

Chemical Name:tert-butyl {1-[4-(5,7-diethyl-3-phenylpyrazolo[1,5-a]pyrimidin-2-yl)phenyl]cyclobutyl}carbamate
CAS No.:1447274-39-6
Molecular Formula:C₃₁H₃₆N₄O₂
Molecular Weight:496.652
Hs Code.:

Synonyms:tert-butyl {1-[4-(5,7-diethyl-3-phenylpyrazolo[1,5-a]pyrimidin-2-yl)phenyl]cyclobutyl}carbamate

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Chemical Property of tert-butyl {1-[4-(5,7-diethyl-3-phenylpyrazolo[1,5-a]pyrimidin-2-yl)phenyl]cyclobutyl}carbamate

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Technology Process of tert-butyl {1-[4-(5,7-diethyl-3-phenylpyrazolo[1,5-a]pyrimidin-2-yl)phenyl]cyclobutyl}carbamate

There total 7 articles about tert-butyl {1-[4-(5,7-diethyl-3-phenylpyrazolo[1,5-a]pyrimidin-2-yl)phenyl]cyclobutyl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1447274-41-0
5,7-diethyl-3-phenylpyrazolo[1,5-a]pyrimidin-2-yl trifluoromethane-sulfonate

: 1447274-42-1
(4-{1-[(tert-butoxycarbonyl)amino]cyclobutyl}phenyl)boronic acid

: 1447274-39-6
tert-butyl {1-[4-(5,7-diethyl-3-phenylpyrazolo[1,5-a]pyrimidin-2-yl)phenyl]cyclobutyl}carbamate

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; caesium carbonate; In N,N-dimethyl-formamide; at 110 ℃; for 0.0111111h; Microwave irradiation;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1447274-39-6
tert-butyl {1-[4-(5,7-diethyl-3-phenylpyrazolo[1,5-a]pyrimidin-2-yl)phenyl]cyclobutyl}carbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydrogencarbonate / dichloromethane; water

1.2: 20 °C / Inert atmosphere

2.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / tetrahydrofuran / 5 h / Reflux

3.1: ammonium acetate; sodium periodate / acetone / 20 °C

4.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; caesium carbonate / N,N-dimethyl-formamide / 0.01 h / 110 °C / Microwave irradiation

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium periodate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; ammonium acetate; potassium acetate; sodium hydrogencarbonate; caesium carbonate; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetone;

Reference yield:

: 1032350-06-3
tert-butyl (1-(4-bromophenyl)cyclobutyl)carbamate

: 1447274-39-6
tert-butyl {1-[4-(5,7-diethyl-3-phenylpyrazolo[1,5-a]pyrimidin-2-yl)phenyl]cyclobutyl}carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / tetrahydrofuran / 5 h / Reflux

2: ammonium acetate; sodium periodate / acetone / 20 °C

3: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; caesium carbonate / N,N-dimethyl-formamide / 0.01 h / 110 °C / Microwave irradiation

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium periodate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; ammonium acetate; potassium acetate; caesium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide; acetone;