C₂₂H₂₉NO₃

Base Information

Chemical Name:C₂₂H₂₉NO₃
CAS No.:1055233-53-8
Molecular Formula:C₂₂H₂₉NO₃
Molecular Weight:355.477
Hs Code.:

C<sub>22</sub>H<sub>29</sub>NO<sub>3</sub>

Synonyms:C₂₂H₂₉NO₃

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Chemical Property of C₂₂H₂₉NO₃

Chemical Property:

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Technology Process of C₂₂H₂₉NO₃

There total 6 articles about C₂₂H₂₉NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1055233-50-5
C₂₀H₂₅NO₃

: 75-03-6
ethyl iodide

: 1055233-53-8
C₂₂H₂₉NO₃

Guidance literature:: C₂₀H₂₅NO₃; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.0833333h; Inert atmosphere;

ethyl iodide; In N,N-dimethyl-formamide; at 20 ℃; for 0.0833333h; Inert atmosphere;

Reference yield:

: 170230-13-4
5-nitro-2-i-propylphenol

: 1055233-53-8
C₂₂H₂₉NO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 1.5 h

2.1: hydrogenchloride; hydrogen / palladium on activated charcoal / methanol; water / 1.5 h / 20 °C

3.1: caesium carbonate / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / toluene / 110 °C / Reflux; Inert atmosphere

4.1: sodium hydride / N,N-dimethyl-formamide / 0.08 h / 20 °C / Inert atmosphere

4.2: 0.08 h / 20 °C / Inert atmosphere

With hydrogenchloride; hydrogen; sodium hydride; potassium carbonate; caesium carbonate; potassium iodide; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; palladium on activated charcoal; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In methanol; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 132475-93-5
2-isopropyl-5-nitroaniline

: 1055233-53-8
C₂₂H₂₉NO₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: sulfuric acid; water; sodium nitrite / 0 - 5 °C

2.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 1.5 h

3.1: hydrogenchloride; hydrogen / palladium on activated charcoal / methanol; water / 1.5 h / 20 °C

4.1: caesium carbonate / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / toluene / 110 °C / Reflux; Inert atmosphere

5.1: sodium hydride / N,N-dimethyl-formamide / 0.08 h / 20 °C / Inert atmosphere

5.2: 0.08 h / 20 °C / Inert atmosphere

With hydrogenchloride; sulfuric acid; water; hydrogen; sodium hydride; potassium carbonate; caesium carbonate; potassium iodide; sodium nitrite; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; palladium on activated charcoal; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In methanol; water; N,N-dimethyl-formamide; toluene;