O-phenyl O-3-pyridinyl thiocarbonate

Base Information

Chemical Name:O-phenyl O-3-pyridinyl thiocarbonate
CAS No.:1242438-11-4
Molecular Formula:C₁₂H₉NO₂S
Molecular Weight:231.275
Hs Code.:

Synonyms:O-phenyl O-3-pyridinyl thiocarbonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-phenyl O-3-pyridinyl thiocarbonate

Chemical Property:

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Technology Process of O-phenyl O-3-pyridinyl thiocarbonate

There total 3 articles about O-phenyl O-3-pyridinyl thiocarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 109-00-2
3-HYDROXYPYRIDINE

: 463-71-8
thiophosgene

: 108-95-2,27073-41-2
phenol

: 1242438-11-4
O-phenyl O-3-pyridinyl thiocarbonate

Guidance literature:: thiophosgene; phenol; With pyridine; In dichloromethane; at 0 - 20 ℃; for 0.25h;

3-HYDROXYPYRIDINE; In dichloromethane; at 20 ℃; for 0.5h;

Reference yield: 75.0%

: 109-00-2
3-HYDROXYPYRIDINE

: 1005-56-7
phenylcarbonochloridothioate

: 1242438-11-4
O-phenyl O-3-pyridinyl thiocarbonate

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃;
DOI:10.1021/jo102467j

Reference yield:

: 108-95-2,27073-41-2
phenol

: 1242438-11-4
O-phenyl O-3-pyridinyl thiocarbonate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / dichloromethane; water / 1 h

2: pyridine / dichloromethane / 20 °C

With pyridine; sodium hydroxide; In dichloromethane; water;
DOI:10.1021/jo102467j