2,6-di-tert-butyl-4-{4-[3,5-di-tert-butyl-4-(3-pyrazol-1-yl-propoxy)phenylsulfanyl]-piperidin-4-ylsulfanyl}phenol

Base Information

Chemical Name:2,6-di-tert-butyl-4-{4-[3,5-di-tert-butyl-4-(3-pyrazol-1-yl-propoxy)phenylsulfanyl]-piperidin-4-ylsulfanyl}phenol
CAS No.:1402048-43-4
Molecular Formula:C₃₉H₅₉N₃O₂S₂
Molecular Weight:666.048
Hs Code.:

Synonyms:2,6-di-tert-butyl-4-{4-[3,5-di-tert-butyl-4-(3-pyrazol-1-yl-propoxy)phenylsulfanyl]-piperidin-4-ylsulfanyl}phenol

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Chemical Property of 2,6-di-tert-butyl-4-{4-[3,5-di-tert-butyl-4-(3-pyrazol-1-yl-propoxy)phenylsulfanyl]-piperidin-4-ylsulfanyl}phenol

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Technology Process of 2,6-di-tert-butyl-4-{4-[3,5-di-tert-butyl-4-(3-pyrazol-1-yl-propoxy)phenylsulfanyl]-piperidin-4-ylsulfanyl}phenol

There total 5 articles about 2,6-di-tert-butyl-4-{4-[3,5-di-tert-butyl-4-(3-pyrazol-1-yl-propoxy)phenylsulfanyl]-piperidin-4-ylsulfanyl}phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1402048-42-3
4-(3,5-di-tert-butyl-4-hydroxyphenylsulfanyl)-4-[3,5-di-tert-butyl-4-(3-pyrazol-1-yl-propoxy)phenylsulfanyl]piperidine-1-carboxylic acid ethyl ester

: 1402048-43-4
2,6-di-tert-butyl-4-{4-[3,5-di-tert-butyl-4-(3-pyrazol-1-yl-propoxy)phenylsulfanyl]-piperidin-4-ylsulfanyl}phenol

Guidance literature:: 4-(3,5-di-tert-butyl-4-hydroxyphenylsulfanyl)-4-[3,5-di-tert-butyl-4-(3-pyrazol-1-yl-propoxy)phenylsulfanyl]piperidine-1-carboxylic acid ethyl ester; With isopropyl alcohol; potassium hydroxide; at 85 ℃; for 24h;

With hydrogenchloride; In water; isopropyl alcohol;

Reference yield:

: 950-59-4
4-hydroxy-3,5-di-tert-butylthiophenol

: 1402048-43-4
2,6-di-tert-butyl-4-{4-[3,5-di-tert-butyl-4-(3-pyrazol-1-yl-propoxy)phenylsulfanyl]-piperidin-4-ylsulfanyl}phenol

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogenchloride / methanol / 20 h / 45 °C

2: potassium carbonate / N,N-dimethyl-formamide / 6 h / 85 °C

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 20 °C

4: sodium hydride / N,N-dimethyl-formamide / 2 h / 20 °C

5: isopropyl alcohol; potassium hydroxide / 24 h / 85 °C

With hydrogenchloride; sodium hydride; potassium carbonate; N-ethyl-N,N-diisopropylamine; isopropyl alcohol; potassium hydroxide; In methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 29976-53-2
N-ethoxycarbonyl-4-piperidone

: 1402048-43-4
2,6-di-tert-butyl-4-{4-[3,5-di-tert-butyl-4-(3-pyrazol-1-yl-propoxy)phenylsulfanyl]-piperidin-4-ylsulfanyl}phenol

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogenchloride / methanol / 20 h / 45 °C

2: potassium carbonate / N,N-dimethyl-formamide / 6 h / 85 °C

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 20 °C

4: sodium hydride / N,N-dimethyl-formamide / 2 h / 20 °C

5: isopropyl alcohol; potassium hydroxide / 24 h / 85 °C

With hydrogenchloride; sodium hydride; potassium carbonate; N-ethyl-N,N-diisopropylamine; isopropyl alcohol; potassium hydroxide; In methanol; dichloromethane; N,N-dimethyl-formamide;