[Ru(η(5)-cyclopentadienyl)(triphenylphosphine)(η(2)(P,O)-Ph2PCH2C(=O)Bu(t))](PF6)*dichloromethane

Base Information

Chemical Name:[Ru(η(5)-cyclopentadienyl)(triphenylphosphine)(η(2)(P,O)-Ph2PCH2C(=O)Bu(t))](PF6)*dichloromethane
CAS No.:198897-39-1
Molecular Formula:CH₂Cl₂*C₄₁H₄₁OP₂Ru*F₆P
Molecular Weight:942.691
Hs Code.:

Synonyms:[Ru(η(5)-cyclopentadienyl)(triphenylphosphine)(η(2)(P,O)-Ph2PCH2C(=O)Bu(t))](PF6)*dichloromethane

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Chemical Property of [Ru(η(5)-cyclopentadienyl)(triphenylphosphine)(η(2)(P,O)-Ph2PCH2C(=O)Bu(t))](PF6)*dichloromethane

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Technology Process of [Ru(η(5)-cyclopentadienyl)(triphenylphosphine)(η(2)(P,O)-Ph2PCH2C(=O)Bu(t))](PF6)*dichloromethane

There total 1 articles about [Ru(η(5)-cyclopentadienyl)(triphenylphosphine)(η(2)(P,O)-Ph2PCH2C(=O)Bu(t))](PF6)*dichloromethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: ammonium hexafluorophosphate

: 32993-05-8
chloro(cyclopentadienyl)bis(triphenylphosphine)ruthenium (II)

: 91222-65-0
3,3-dimethyl-1-(diphenylphosphino)butan-2-one

: 198897-39-1
[Ru(η(5)-cyclopentadienyl)(triphenylphosphine)(η(2)(P,O)-Ph2PCH2C(=O)Bu(t))](PF6)*dichloromethane

Guidance literature:: In methanol; Ar or N2-atmosphere; slight excess of phosphine and NH4PF6, refluxing for 3 h; evapn., stirring with Et2O, collection (filtration), washing (Et2O), extn. (CH2Cl2), filtration, crystn. on addn. of MeOH and Et2O; elem. anal.;
DOI:10.1021/om970513n

Reference yield: 99.0%

: 198897-39-1
[Ru(η(5)-cyclopentadienyl)(triphenylphosphine)(η(2)(P,O)-Ph2PCH2C(=O)Bu(t))](PF6)*dichloromethane

: 198897-56-2
Ru(η(5)-cyclopentadienyl)(triphenylphosphine)(η(2)(P,O)-Ph2PCH=C(O)Bu(t))

Guidance literature:: With K₂CO₃; In methanol; Ar or N2-atmosphere; excess of K2CO3, stirring overnight; collection (filtration), washing (H2O, MeOH); elem. anal.;
DOI:10.1021/om970513n

Reference yield: 82.0%

: 198897-39-1
[Ru(η(5)-cyclopentadienyl)(triphenylphosphine)(η(2)(P,O)-Ph2PCH2C(=O)Bu(t))](PF6)*dichloromethane

: 3923-52-2
1,1-diphenyl-2-propyn-1-ol

: [Ru(=C=C=CPh2)(η(5)-cyclopentadienyl)(triphenylphosphine)(η(1)(P)-Ph2PCH2C(=O)Bu(t))](PF6)

Guidance literature:: In methanol; Ar or N2-atmosphere; excess of alkyne, refluxing for 6 h; evapn., washing (Et2O), recrystn. (CH2Cl2:Et2O); elem. anal.;
DOI:10.1021/om970513n