10-deacetyl-7,10-bis<(2,2,2-trichloroethoxy)carbonyl>-2-(hexahydro)baccatin III

Base Information

Chemical Name:10-deacetyl-7,10-bis<(2,2,2-trichloroethoxy)carbonyl>-2-(hexahydro)baccatin III
CAS No.:158660-67-4
Molecular Formula:C₃₅H₄₄Cl₆O₁₄
Molecular Weight:901.444
Hs Code.:

Synonyms:10-deacetyl-7,10-bis<(2,2,2-trichloroethoxy)carbonyl>-2-(hexahydro)baccatin III

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 10-deacetyl-7,10-bis<(2,2,2-trichloroethoxy)carbonyl>-2-(hexahydro)baccatin III

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Technology Process of 10-deacetyl-7,10-bis<(2,2,2-trichloroethoxy)carbonyl>-2-(hexahydro)baccatin III

There total 2 articles about 10-deacetyl-7,10-bis<(2,2,2-trichloroethoxy)carbonyl>-2-(hexahydro)baccatin III which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 158660-66-3
10-deacetyl-2-(hexahydro)baccatin III

: 17341-93-4
2,2,2-Trichloroethyl chloroformate

: 158660-67-4
10-deacetyl-7,10-bis<(2,2,2-trichloroethoxy)carbonyl>-2-(hexahydro)baccatin III

Guidance literature:: With pyridine; at 80 ℃; for 0.5h;
DOI:10.1021/jm00042a013

Reference yield:

: 32981-86-5,172018-16-5
10-deacetylbaccatin III

: 158660-67-4
10-deacetyl-7,10-bis<(2,2,2-trichloroethoxy)carbonyl>-2-(hexahydro)baccatin III

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / H₂ / 5percent Rh/C / methanol / 24 h / 35 °C / 25857.4 Torr

2: 74 percent / pyridine / 0.5 h / 80 °C

With pyridine; hydrogen; Rh on carbon; In methanol;
DOI:10.1021/jm00042a013